A novel strategy to synthesize cobalt hydroxide and Co3O4 nanowires

被引：96

作者：

Mahmoud, Waleed E. ^{[1
,2
]}

Al-Agel, F. A. ^{[1
]}

机构：

[1] King Abdulaziz Univ, Fac Sci, Dept Phys, Jeddah, Saudi Arabia

[2] Suez Canal Univ, Fac Sci, Dept Phys, Ismailia, Egypt

来源：

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS | 2011年 / 72卷 / 07期

关键词：

Nanostructures; Chemical synthesis; Electron microscopy; Crystal structure; HYDROTHERMAL SYNTHESIS; COO; NANORODS; NANOSTRUCTURES; FABRICATION; CHEMISTRY; OXYGEN; FILMS;

D O I：

10.1016/j.jpcs.2011.04.014

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Cobalt hydroxide ultra fine nanowires were prepared by a facile hydrothermal route using hydrogen peroxide. This method provides a simple, low cost, and large-scale route to produce beta-cobalt hydroxide nanowires with an average diameter of 5 nm and a length of ca. 10 mu m, which show a predominant well-crystalline hexagonal brucite-like phase. Their thermal decomposition produced highly uniform nanowires of cobalt oxide (Co3O4) under temperature 500 degrees C in the presence of oxygen gas. The produced cobalt oxide was characterized by X-ray diffraction, transmission electronic microscopy, and selected-area electron diffraction. The results indicated that cobalt oxide nanowires with an average diameter of 10 nm and a length of ca. 600 nm have been formed, which show a predominant well-crystalline cubic face-centered like phase. (C) 2011 Elsevier Ltd. All rights reserved.

引用

页码：904 / 907

页数：4

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