Crystal growth of some amino acids in gel: Crystallization of DL-serine and its characterization

被引：0

作者：

Ramachandran, E ^{[1
]}

Natarajan, S

机构：

[1] Thiruvalluvar Coll, Dept Phys, Papanasam 627425, India

[2] Madurai Kamaraj Univ, Dept Phys, Madurai 625021, Tamil Nadu, India

来源：

INDIAN JOURNAL OF PURE & APPLIED PHYSICS | 2005年 / 43卷 / 05期

关键词：

DL-serine; amino acid; gel growth; XRD; TGA/DTA;

D O I：

暂无

中图分类号：

O4 [物理学];

学科分类号：

0702 ;

摘要：

DL-serine (C3H7NO3) a neutral, genetically coded amino acid was crystallized in silica gel under suitable pH conditions by reduction of solubility method. The gel grown DL-serine crystals were characterized by density determination and X-ray powder diffraction. Fourier transform infrared spectroscopic studies and thermogravimetric analysis were also made.

引用

页码：372 / 376

页数：5

共 15 条

[1] THE FINAL PHASES OF CALCIUM AND MAGNESIUM PHOSPHATES PRECIPITATED FROM SOLUTIONS OF HIGH TO MEDIUM CONCENTRATION [J].

ABBONA, F ;

MADSEN, HEL ;

BOISTELLE, R .

JOURNAL OF CRYSTAL GROWTH, 1988, 89 (04) :592-602

[2] REFINEMENTS OF CRYSTAL-STRUCTURES OF DL-SERINE AND ANHYDROUS L-SERINE [J].

KISTENMACHER, TJ ;

RAND, GA ;

MARSH, RE .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS, 1974, 30 (NOV15) :2573-2578

[3]

Laugier J., 2003, ENSP LAB MATERIAUXD, V46, P38042

[4] GEL GROWTH OF SINGLE-CRYSTALS OF ALPHA-GLYCINE, L-THREONINE AND N-GLYCYLGLYCINE [J].

NATARAJAN, S ;

DEVADOSS, HA ;

ALWAN, K .

CRYSTAL RESEARCH AND TECHNOLOGY, 1988, 23 (10-11) :1343-1346

[5]

NATARAJAN S, 1997, CRYST RES TECHNOL, V32, P551

[6]

PHYLLIS B, 2000, PRESCRIPTION NUTRION

[7] Crystal growth of some urinary stone constituents: III. In-vitro crystallization of L-cystine and its characterization [J].

Ramachandran, E ;

Natarajan, S .

CRYSTAL RESEARCH AND TECHNOLOGY, 2004, 39 (04) :308-312

[8] Crystal growth of some urinary stone constituents: II. In-vitro crystallization of hippuric acid. [J].

Ramachandran, E ;

Natarajan, S .

CRYSTAL RESEARCH AND TECHNOLOGY, 2002, 37 (12) :1274-1279

[9]

Ramachandran E, 2002, CRYST RES TECHNOL, V37, P1160, DOI 10.1002/1521-4079(200211)37:11<1160::AID-CRAT1160>3.0.CO

[10]

2-K

← 1 2 →