A simple method to synthesize Ba0.6Sr0.4TiO3 nano-powders through high-energy ball-milling

被引:18
作者
Liu, Cheng [1 ]
Liu, Peng [1 ]
Lu, Xiao-gang [2 ]
Gao, Chang-jie [2 ]
Zhu, Gang-qiang [1 ]
Chen, Xiao-ming [1 ]
机构
[1] Shaanxi Normal Univ, Coll Phys & Informat Technol, Xian 710062, Peoples R China
[2] China Ordnance Ind Grp Corp, Inst 206, Xian 710100, Peoples R China
基金
中国国家自然科学基金;
关键词
BST; Powder preparation; Thermal analysis; Microstructure; BARIUM-STRONTIUM-TITANATE; LOW-TEMPERATURE SYNTHESIS; DIELECTRIC-PROPERTIES; CERAMIC COMPOSITES; MICROSTRUCTURE; NANOPOWDERS;
D O I
10.1016/j.powtec.2011.05.010
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
In this study, we fabricated Ba0.6Sr0.4TiO3 (BST) powders via a high-energy ball-milling (HEBM) method. The processing parameters were optimized to obtain an optimum synthesis condition. BST nano-powders (with a mean grain size of 475 nm) were derived from the precursor milled at 400/800 rpm for 5 h and calcined at 1000 degrees C for 2 h. This synthesis temperature was much lower than that required by traditional solid state reaction. It was suggested that HEBM is a simple and practical route to synthesize BST nano-powders. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:299 / 302
页数:4
相关论文
共 26 条
[21]  
SENGUPTA L, 1996, Patent No. 5486491
[22]   Novel ferroelectric materials for phased array antennas [J].
Sengupta, LC ;
Sengupta, S .
IEEE TRANSACTIONS ON ULTRASONICS FERROELECTRICS AND FREQUENCY CONTROL, 1997, 44 (04) :792-797
[23]   Breakthrough advances in low loss, tunable dielectric materials [J].
Sengupta, LC ;
Sengupta, S .
MATERIALS RESEARCH INNOVATIONS, 1999, 2 (05) :278-282
[24]   Low-temperature sintering of (Ba0.6Sr0.4)TiO3 [J].
Valant, M ;
Suvorov, D .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2004, 87 (07) :1222-1226
[25]   Low-temperature synthesis of superfine barium strontium titanate powder by the citrate method [J].
Zhang, Xiao-Fei ;
Xu, Qing ;
Huang, Yu-Heng ;
Liu, Han-Xing ;
Huang, Duan-Ping ;
Zhang, Feng .
CERAMICS INTERNATIONAL, 2010, 36 (04) :1405-1409
[26]   A novel method for preparation of barium strontium titanate nanopowders [J].
Zuo, X. H. ;
Deng, X. Y. ;
Chen, Y. ;
Ruan, M. ;
Li, W. ;
Liu, B. ;
Qu, Y. ;
Xu, B. .
MATERIALS LETTERS, 2010, 64 (10) :1150-1153