Lateral structural variations in thin cellulose layers investigated by microbeam grazing incidence small-angle X-ray scattering

被引：13
作者：
Roth, SV
Artus, GRJ
Rankl, M
Seeger, S
Burghammer, M
Riekel, C
Müller-Buschbaum, P
机构：
[1] European Synchrotron Radiat Facil, F-38043 Grenoble 9, France
[2] DESY, HASYLAB, D-22603 Hamburg, Germany
[3] Univ Zurich, Inst Chem Phys, CH-8057 Zurich, Switzerland
[4] Tech Univ Munich, Dept Phys, D-85748 Garching, Germany
来源：
PHYSICA B-CONDENSED MATTER | 2005年 / 357卷 / 1-2期
关键词：
biological coating; thin film; GTSAXS; microbeam; Langmuir Blodgett; MULTILAYERS;
D O I：
10.1016/j.physb.2004.11.054
中图分类号：
O469 [凝聚态物理学];
学科分类号：
070205 ;
摘要：
The Langmuir-Blodgett technique is a powerful tool to obtain large-scale thin films. We investigate a thin layer of modified cellulose by atomic force microscopy and microbeam grazing-incidence small angle X-ray scattering. We probe the lateral nanostructure of the as-prepared cellulose layer. The results indicate a lateral structural variation in the arrangement of the cellulose molecules parallel to the dipping direction. These variations occur on a length scale on the order of 100 pm. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码：190 / 192
页数：3
相关论文
共 8 条
[1]   NONSPECULAR X-RAY REFLECTION FROM ROUGH MULTILAYERS [J].
HOLY, V ;
BAUMBACH, T .
PHYSICAL REVIEW B, 1994, 49 (15) :10668-10676
[2]   Combined scanning microdiffraction and micro small-angle scattering at the microfocus beamline ID13 (ESRF) [J].
Müller, M ;
Burghammer, M ;
Riekel, C .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2001, 467 :958-961
[3]   Multiple-scaled polymer surfaces investigated with micro-focus grazing-incidence small-angle X-ray scattering [J].
Müller-Buschbaum, P ;
Roth, SV ;
Burghammer, M ;
Diethert, A ;
Panagiotou, P ;
Riekel, C .
EUROPHYSICS LETTERS, 2003, 61 (05) :639-645
[4]   Surface tension properties of surface-coatings for application in biodiagnostics determined by contact angle measurements [J].
Rankl, M ;
Laib, S ;
Seeger, S .
COLLOIDS AND SURFACES B-BIOINTERFACES, 2003, 30 (03) :177-186
[5]  
RANKL M, 2004, THESIS U ZURICH
[6]   Self-assembled gradient nanoparticle-polymer multilayers investigated by an advanced characterization method:: microbeam grazing incidence x-ray scattering [J].
Roth, SV ;
Burghammer, M ;
Riekel, C ;
Müller-Buschbaum, P ;
Diethert, A ;
Panagiotou, P ;
Walter, H .
APPLIED PHYSICS LETTERS, 2003, 82 (12) :1935-1937
[7]   ULTRATHIN LAYERS AND SUPRAMOLECULAR ARCHITECTURE OF ISOPENTYLCELLULOSE [J].
SCHAUB, M ;
FAKIROV, C ;
SCHMIDT, A ;
LIESER, G ;
WENZ, G ;
WEGNER, G ;
ALBOUY, PA ;
WU, H ;
FOSTER, MD ;
MAJKRZAK, C ;
SATIJA, S .
MACROMOLECULES, 1995, 28 (04) :1221-1228
[8]   ORIGIN OF ORIENTATION PHENOMENA OBSERVED IN LAYERED LANGMUIR-BLODGETT STRUCTURES OF HAIRY-ROD POLYMERS [J].
SCHWIEGK, S ;
VAHLENKAMP, T ;
XU, YZ ;
WEGNER, G .
MACROMOLECULES, 1992, 25 (09) :2513-2525
1