A third polymorph of N,N′-bis(pyridin-2-yl)benzene-1,4-diamine

被引:5
|
作者
Wicher, Barbara [1 ]
Gdaniec, Maria [1 ]
机构
[1] Adam Mickiewicz Univ Poznan, Fac Chem, PL-60780 Poznan, Poland
关键词
D O I
10.1107/S1600536811044539
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
A third polymorph of the title compound, C(16)H(14)N(4), has been obtained. The molecule adopts a non-planar conformation with an E configuration at the two partially double exo C(sic)N bonds of the 2-pyridylamine units. Like in the triclinic form [Bensemann et al. (2002). New J. Chem. 26, 448-456], the recognition process between 2-pyridylamine units takes place through formation of a cyclic R(2)(2) (8) hydrogen-bond motif, leading to the creation of tapes parallel to [001].
引用
收藏
页码:O3095 / U1940
页数:10
相关论文
共 50 条
  • [31] Synthesis, crystal and molecular structures of 1D and 2D supramers of copper(II) with N,N′-{bis(pyridin-2-yl) benzylidenel butane-1,4-diamine
    Rahaman, Sk Hafijur
    Bose, Doyel
    Ghosh, Rajarshi
    Mostafa, Golam
    Fun, Hoong-Kun
    Ghosh, Barindra K.
    STRUCTURAL CHEMISTRY, 2007, 18 (02) : 237 - 244
  • [32] Crystal structure of N-1-phenyl-N-4-[(E)-(pyren-1-yl)methylidene]benzene-1,4-diamine
    Faizi, Md. Serajul Haque
    Prisyazhnaya, Elena V.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 261 - +
  • [33] N,N′-Dimethyl-N,N′-bis(pyridin-2-yl)methanediamine
    Lee, Moon-Sun
    Yoon, Minyoung
    Yang, O-bong
    Lee, Dong-Heon
    Park, Gyungse
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3226 - U828
  • [34] Crystal Structure and Spectroscopic Characterization of Zinc(II) and Mercury(II) Complexes of N-(Pyridin-2-ylmethylene)benzene-1,4-diamine
    Marjani, Katayoun
    Asgarian, Jafar
    Mousavi, Mohsen
    Amani, Vahid
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2009, 635 (11): : 1633 - 1637
  • [35] catena-Poly[[(nitrato-κ2 O,O')silver(I)]-μ-N,N'-bis(3-pyridylmethylidene)benzene-1,4-diamine]
    Liu, Yong-Hao
    Xu, Quan
    Han, Zhi-You
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M903 - U423
  • [36] catena-Poly[[dichloridomercury(II)]-μ-1,4-bis[(pyridin-2-yl)methoxy]benzene-κ2N:N′]
    Liu, Ying
    Zhang, Hong-Sen
    Hu, Ming-Xing
    Hou, Guang-Feng
    Gao, Jin-Sheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1427 - U1188
  • [37] N,N′-bis(2-pyridyl)benzene-1,2-diamine
    Gdaniec, M
    Bensemann, I
    Polonski, T
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 : O215 - O216
  • [38] N,N′-bis(2-tosylaminobenzylidene)-benzene-1,2-diamine
    Mahía, J
    Maestro, MA
    Vázquez, M
    Bermejo, MR
    González, AM
    Maneiro, M
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2000, 56 : 492 - 493
  • [39] N-[4-(1-Methyl-1H-imidazol-2-yl)-2,4 '-bipyridin-2-' yl]benzene-1,4-diamine
    Zinad, Dhafer S.
    AL-Duhaidahaw, Dunya L.
    Al-Amiery, Ahmed
    Kadhum, Abdul Amir H.
    MOLBANK, 2018, (04)
  • [40] Characterization and tunneling conductance spectra of N,N′-bis (9H-fluoren-9-ylidene)benzene-1,4-diamine thin films on graphite
    Xin, Hongliang
    Li, Zhuomin
    He, Tianxian
    Miao, Xinrui
    Deng, Wenli
    MATERIALS CHEMISTRY AND PHYSICS, 2010, 121 (03) : 572 - 577