The crystal and molecular structure of 6,8,15,16b,16c,17-hexahydro-16b,16c-diphenyl-7H,16H-6a,7a,15a,16a-tetraazanaphtho[5,6]azulano[2,1,8,-ij]naptho[f]azulene-7,16-dione

被引:2
|
作者
Bosman, WP
Smits, JMM
deGelder, R
Reek, JNH
Nolte, RJM
机构
[1] UNIV NIJMEGEN,DEPT ORGAN CHEM,NIJMEGEN SON RES CTR,NL-6525 ED NIJMEGEN,NETHERLANDS
[2] UNIV NIJMEGEN,DEPT INORGAN CHEM,NIJMEGEN SON RES CTR,NL-6525 ED NIJMEGEN,NETHERLANDS
关键词
crystal structure; receptor; clip shaped molecule;
D O I
10.1007/BF01677102
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal and molecular structure of a clip containing molecule is described. The structure was solved by vector search methods and refined by least squares methods to R(1) = 0.0768 [I > 2 sigma(I)]. Crystal data: C40H30N4O2 . HCCl3, triclinic, space group P (1) over bar, a = 9.302(2), b = 12.981(2), c = 15.765(2)Angstrom, alpha = 65.91(2)degrees, beta = 76.40(2)degrees, gamma = 80.15(1)degrees, V = 1682.9(4)Angstrom(3), Z = 2.
引用
收藏
页码:365 / 368
页数:4
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