Simple calibrated merging of gas chromatography capillary column temperature-programmed retention-index compilations

被引:19
作者
Richmond, R
机构
[1] Structure Elucidation Group, Preclinical Research Department, Sandoz Pharma AG
关键词
retention indices; temperature-programmed retention indices;
D O I
10.1016/0021-9673(95)00924-8
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Experimental calibration methods were used to generate gas chromatographic retention index offset plots to allow the comparison of separate temperature-programmed retention index datasets, for the eventual purpose of merging them. The 8 degrees C/min on an OV-1 stationary phase subset of the Sadtler Standard Gas Chromatography Retention Index Library was used as an initial model. After merging, individual experimental search windows were assigned to each of the structures from the incorporated datasets.
引用
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页码:229 / 234
页数:6
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