Synthesis of boron nitride from boron containing poly(vinyl alcohol) as ceramic precursor

被引:14
作者
Das, M. [1 ]
Ghatak, S. [1 ]
机构
[1] CSIR Cent Glass & Ceram Res Inst, Bioceram & Coating Div, Kolkata 700032, India
关键词
Polyvinyl alcohol; preceramic polymer; boron nitride; CHEMICAL-VAPOR-DEPOSITION; CARBIDE; FILMS; BLUE; BN;
D O I
10.1007/s12034-011-0248-4
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A ceramic precursor, prepared by condensation reaction from poly(vinyl alcohol) (PVA) and boric acid (H3BO3) in 1:1, 2:1 and 4:1 molar ratios, was synthesized as low temperature synthesis route for boron nitride ceramic. Samples were pyrolyzed at 850A degrees C in nitrogen atmosphere followed by characterization using Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD).
引用
收藏
页码:99 / 102
页数:4
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