Microstructure and Phase Composition of the Two-Phase Ceramic Synthesized from Titanium Oxide and Zinc Oxide

被引:4
作者
Zeer, Galina M. [1 ]
Zelenkova, Elena G. [1 ]
Nikolaeva, Natalia S. [1 ]
Zharkov, Sergey M. [1 ,2 ]
Abkaryan, Artur K. [1 ]
Mikheev, Anatoly A. [3 ]
机构
[1] Siberian Fed Univ, Krasnoyarsk 660041, Russia
[2] RAS, SB, KSC, Kirensky Inst Phys,Fed Res Ctr, Krasnoyarsk 660036, Russia
[3] Siberian State Aerosp Univ, Krasnoyarsk 660014, Russia
基金
俄罗斯基础研究基金会;
关键词
Nanopowders; Titanium oxide; Zinc oxide; Solid phase reaction; Ceramic; ZNO; FABRICATION;
D O I
10.2298/SOS1802173Z
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
We have made investigations of the phase formation and microstructure on the ceramics obtained from a starting nanopowder mixture with the weight ratio ZnO: TiO2 = 4 : 1. Ceramic is obtained at different sintering temperatures, namely, 948, 1223 and 1473 K. Using the characterization methods of electron microscopy, energy dispersive microanalysis and X-ray diffraction phase analysis it has been shown that the ceramics structure is consisted of two dispersed phases of Zn2TiO4 and ZnO with the grain sizes being in range 0,5-1 mu m. It has been found also that, at ceramic's sintering temperature of 1223 K, the solid phase interactions are completed with the structure ZnO : Zn2TiO4 approximate to 1 : 1,5 phase ratio.
引用
收藏
页码:173 / 181
页数:9
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