Electrochemical characterization of nano-sized gold electrodes fabricated by nano-lithography

被引:14
作者
Kleijn, Steven E. F. [1 ]
Yanson, Alexei I. [1 ]
Koper, Marc T. M. [1 ]
机构
[1] Leiden Univ, Leiden Inst Chem, NL-2300 RA Leiden, Netherlands
关键词
Nano-electrodes; Nanolithography; Gold electrodes; HIGH-MASS TRANSPORT; MICROELECTRODE ARRAYS; DEPOSITION; OXIDATION; ELECTROCATALYSIS; NANOELECTRODES; PLATINUM; SILICON; CARBON; FILMS;
D O I
10.1016/j.jelechem.2011.11.022
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
We report the lithographical fabrication of Au nanoelectrodes, with a geometrical surface area down to 160 nm x 1 mu m. The geometrical surface area of the electrodes is verified using electron microscopy and by electrochemistry through the diffusion limited current of reversible redox couples. Moreover, the electrochemically active surface area of the electrodes is determined from the charges transferred in blank voltammetry. We believe these reproducible nanoelectrodes are well suited for use as probes in nano-electrochemistry research. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码:19 / 24
页数:6
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