C4 Dissymmetric resorcinarene derivatives: synthesis, crystal structure and micelle formation

被引：5
|
作者：
McIldowie, Matthew J. [1 ,2 ]
Mocerino, Mauro [1 ,2 ]
Ogden, Mark I. [1 ,2 ]
Skelton, Brian W. [3 ,4 ]
White, Allan H. [3 ]
机构：
[1] Curtin Univ, Dept Chem, Bentley, WA 6845, Australia
[2] Curtin Univ, Nanochem Res Inst, Bentley, WA 6845, Australia
[3] Univ Western Australia, Sch Chem & Biochem, Crawley, WA 6009, Australia
[4] Univ Western Australia, Ctr Microscopy Characterisat & Anal, Crawley, WA 6009, Australia
来源：
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 2015年 / 82卷 / 1-2期
关键词：
Crystal structure; Resorcinarene; C-4; Dissymmetry; Micelles; CAPILLARY-ELECTROPHORESIS; CALIXARENES; SEPARATIONS; SURFACTANTS; AMINES;
D O I：
10.1007/s10847-015-0525-8
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The synthesis of a C-4 dissymmetric resorcinarene tetracarboxylic acid derivative and determination of its critical micelle concentration is reported. The tetrahydroxy derivative was prepared by reduction of the tetra-acid. The low-temperature single crystal X-ray structure of the methyl ester derivative of the tetra-acid is also reported. This crystallised with two independent molecules of similar boat (flattened cone) conformation within the asymmetric unit.
引用
收藏
页码：47 / 51
页数：5
相关论文
共 50 条
  • [41] Synthesis and structure of an unusual complex formed between 1,2-bis(3′-pyridyl)ethyne and C-methyl calix[4]resorcinarene
    Ivan Georgiev
    Eric Bosch
    Charles L. Barnes
    Journal of Chemical Crystallography, 2004, 34 : 859 - 864
  • [42] Synthesis and crystal structure of 2-debenzoyl and 4-deacetyl 1-deoxybaccatin VI derivatives
    Lin, HX
    Jiang, Y
    Chen, JM
    Chen, JK
    Chen, MQ
    JOURNAL OF MOLECULAR STRUCTURE, 2005, 738 (1-3) : 59 - 65
  • [43] Synthesis, crystal structure and spectroscopic characterisation of two naphthylmethyl derivatives tolylazoimidazole
    Jiang, Shuang-Shuang
    Qiu, Jiang-Hong
    Jin, Chuan-Ming
    JOURNAL OF CHEMICAL RESEARCH, 2014, (07) : 414 - 417
  • [44] Synthesis and Crystal Structure Studies of Three N-Phenylphthalimide Derivatives
    Rauf, Muhammad Khawar
    Mushtaq, Rabia
    Badshah, Amin
    Kingsford-Adaboh, Robert
    Harrison, Jerry Joe Ebow Kingsley
    Ishida, Hiroyuki
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2013, 43 (03) : 144 - 150
  • [45] Thiourea and thioether derivatives of sorafenib: synthesis, crystal structure, and antiproliferative activity
    Jianwen Yao
    Jing Chen
    Zuopeng He
    Wei Sun
    Hao Fang
    Wenfang Xu
    Medicinal Chemistry Research, 2013, 22 : 3959 - 3968
  • [46] Synthesis, crystal structure, and antinociceptive effects of some new riluzole derivatives
    Wu, Xiang-Long
    Liu, Liu
    Li, You-Jia
    Luo, Jie
    Gai, Dong-Wei
    Lu, Ting-Li
    Mei, Qi-Bing
    MEDICINAL CHEMISTRY RESEARCH, 2018, 27 (05) : 1374 - 1383
  • [47] Synthesis, crystal structure, and antinociceptive effects of some new riluzole derivatives
    Xiang-Long Wu
    Liu Liu
    You-Jia Li
    Jie Luo
    Dong-Wei Gai
    Ting-Li Lu
    Qi-Bing Mei
    Medicinal Chemistry Research, 2018, 27 : 1374 - 1383
  • [48] Thiourea and thioether derivatives of sorafenib: synthesis, crystal structure, and antiproliferative activity
    Yao, Jianwen
    Chen, Jing
    He, Zuopeng
    Sun, Wei
    Fang, Hao
    Xu, Wenfang
    MEDICINAL CHEMISTRY RESEARCH, 2013, 22 (08) : 3959 - 3968
  • [49] Synthesis, crystal structure and biological activities of 2-substituted-3-aryl-4-thiazolidinone(thiazolidinethione) derivatives
    Sun, Xiao-Jun
    Dong, Wei-Li
    Zhao, Wei-Guang
    Li, Zheng-Ming
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2007, 27 (11) : 1374 - 1380
  • [50] SYNTHESIS AND CRYSTAL-STRUCTURE OF LIHSO4
    KEMNITZ, E
    WERNER, C
    WORZALA, H
    TROJANOV, S
    STRUTSCHKOV, YT
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1995, 621 (04): : 675 - 678
12345