C4 Dissymmetric resorcinarene derivatives: synthesis, crystal structure and micelle formation

被引：5
作者：
McIldowie, Matthew J. [1 ,2 ]
Mocerino, Mauro [1 ,2 ]
Ogden, Mark I. [1 ,2 ]
Skelton, Brian W. [3 ,4 ]
White, Allan H. [3 ]
机构：
[1] Curtin Univ, Dept Chem, Bentley, WA 6845, Australia
[2] Curtin Univ, Nanochem Res Inst, Bentley, WA 6845, Australia
[3] Univ Western Australia, Sch Chem & Biochem, Crawley, WA 6009, Australia
[4] Univ Western Australia, Ctr Microscopy Characterisat & Anal, Crawley, WA 6009, Australia
来源：
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 2015年 / 82卷 / 1-2期
关键词：
Crystal structure; Resorcinarene; C-4; Dissymmetry; Micelles; CAPILLARY-ELECTROPHORESIS; CALIXARENES; SEPARATIONS; SURFACTANTS; AMINES;
D O I：
10.1007/s10847-015-0525-8
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The synthesis of a C-4 dissymmetric resorcinarene tetracarboxylic acid derivative and determination of its critical micelle concentration is reported. The tetrahydroxy derivative was prepared by reduction of the tetra-acid. The low-temperature single crystal X-ray structure of the methyl ester derivative of the tetra-acid is also reported. This crystallised with two independent molecules of similar boat (flattened cone) conformation within the asymmetric unit.
引用
收藏
页码：47 / 51
页数：5
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