Caking of amorphous powders - Material aspects, modelling and applications

被引:97
作者
Hartmann, Markus [1 ]
Palzer, Stefan [2 ]
机构
[1] Nestle Prod Technol Ctr, D-78224 Singen, Germany
[2] Nestle Res Ctr, CH-1000 Lausanne 26, Switzerland
关键词
Caking; Amorphous powders; Sintering; Time consolidation; GLASS-TRANSITION; TEMPERATURE; AGGLOMERATION; MECHANISMS; STRENGTH; FORCES;
D O I
10.1016/j.powtec.2010.04.014
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Caking of powders and bulk granules and adhesion of powders on equipment surfaces is a serious problem in the food, chemical and pharmaceutical industries. While caking of crystalline particles is tackled only briefly, this publication deals mainly with caking of water-soluble amorphous particles. Caking of amorphous particles starts with stickiness of the powder surface and can result in a collapse of the powder structure. The powder bulk turns from a free flowable powder bulk composed of single particles into a massive block. The material aspects (hygrocapacity, hygrosensitivity and viscosity) of water-soluble amorphous materials and sintering are discussed. The increase of the sinter bridges during caking could be modelled through the known sinter equations and measured by carrying out experiments in a ring shear cell. The calculated sinter bridge diameter could be correlated with the strength of the caked powder bulk measured in a ring shear tester. (c) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:112 / 121
页数:10
相关论文
共 38 条
[1]   CAKING PHENOMENA IN AMORPHOUS FOOD POWDERS [J].
AGUILERA, JM ;
DELVALLE, JM ;
KAREL, M .
TRENDS IN FOOD SCIENCE & TECHNOLOGY, 1995, 6 (05) :149-155
[2]   EFFECT OF WATER-CONTENT ON THE GLASS-TRANSITION AND CAKING OF FISH-PROTEIN HYDROLYZATES [J].
AGUILIERA, JM ;
LEVI, G ;
KAREL, M .
BIOTECHNOLOGY PROGRESS, 1993, 9 (06) :651-654
[3]   Formation and growth of crystal bridges in bulk solids [J].
Broeckel, Ulrich ;
Wahl, Michael ;
Kirsch, Roman ;
Feise, Hermann J. .
CHEMICAL ENGINEERING & TECHNOLOGY, 2006, 29 (06) :691-695
[4]   Adsorption of gases in multimolecular layers [J].
Brunauer, S ;
Emmett, PH ;
Teller, E .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1938, 60 :309-319
[5]   MECHANISM OF STICKINESS IN HYGROSCOPIC, AMORPHOUS POWDERS [J].
DOWNTON, GE ;
FLORESLUNA, JL ;
KING, CJ .
INDUSTRIAL & ENGINEERING CHEMISTRY FUNDAMENTALS, 1982, 21 (04) :447-451
[6]  
Frenkel J., 1945, J PHYS-USSR, V9, P385
[7]   IDEAL COPOLYMERS AND THE 2ND-ORDER TRANSITIONS OF SYNTHETIC RUBBERS .1. NON-CRYSTALLINE COPOLYMERS [J].
GORDON, M ;
TAYLOR, JS .
JOURNAL OF APPLIED CHEMISTRY, 1952, 2 (09) :493-500
[8]   The London - Van Der Waals attraction between spherical particles [J].
Hamaker, HC .
PHYSICA, 1937, 4 :1058-1072
[9]  
Jenike A.W., 1959, ASME Journal of Applied Mechanics, VE26, P599
[10]   Mathematical model for prediction of glass transition temperature of fruit powders [J].
Khalloufi, S ;
El-Maslouhi, Y ;
Ratti, C .
JOURNAL OF FOOD SCIENCE, 2000, 65 (05) :842-848