High-Temperature Synthesis of Cr-Mo-Al-C Materials

被引:2
作者
Gorshkov, V. A. [1 ]
Kovalev, D. Yu [1 ]
Boyarchenko, O. D. [1 ]
Sychev, A. E. [1 ]
机构
[1] Russian Acad Sci, Merzhanov Inst Struct Macrokinet & Mat Sci, Chernogolovka 142432, Moscow Oblast, Russia
关键词
self-propagating high-temperature synthesis; cast materials; MAX phase; solid solutions; carbides; phase composition; microstructure; MAX-PHASE COMPOUNDS; CERAMICS; SHS;
D O I
10.1134/S0020168521120074
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We report high-temperature synthesis of cast composite materials in the Cr-Mo-Al-C system. (Cr1-xMox)(2)AlC -based materials have been prepared for the first time from a Cr2O3 + MoO3 + Al + C powder mixture by self-propagating high-temperature synthesis in the combustion regime. The synthesis was carried out in a 3-L reactor at an argon pressure of 5 MPa. The composition of the starting mixture has been shown to influence the phase composition and structure of the synthesis products. The synthesized materials contain (Cr1-xMox)(2)AlC and (MoxCr1-x)(3)Al2C phases of variable composition and secondary chromium and molybdenum carbides and intermetallic phases. The materials have been characterized by X-ray diffraction and electron microscopy.
引用
收藏
页码:1300 / 1306
页数:7
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