Synthesis of new carbazole-containing fullerenopyrrolidines

被引：2

作者：

Gubskaya, VP ^{[1
]}

Ovechkina, EV ^{[1
]}

Yanilkin, VV ^{[1
]}

Morozov, VI ^{[1
]}

Nastapova, NV ^{[1
]}

Zverev, VV ^{[1
]}

Azancheev, NM ^{[1
]}

Nuretdinov, IA ^{[1
]}

机构：

[1] Russian Acad Sci, AE Arbuzov Inst Organ & Phys Chem, Kazan Res Ctr, Kazan 420088, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2005年 / 54卷 / 02期

基金：

俄罗斯基础研究基金会;

关键词：

fullerene C-60; fullerenopyrrolidines; 3-formyl-9-isoamylcarbazole; 3,6-diformyl-9-isoamylcarbazole; HPLC; H-1 and C-13 NMR spectroscopy; UV spectroscopy; IR spectroscopy; MALDI-TOF mass spectrometry; cyclic voltammetry; ESR spectroscopy;

D O I：

10.1007/s11172-005-0256-x

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reactions of fullerene C-60 and N-methylglycine with 3-formyl-9-isoamylcarbazole or 3,6-diformyl-9-isoamylcarbazole afforded new carbazole-containing fullerenopyrrolidines. Their structures were established by spectroscopic methods. Electrochemical reduction and oxidation of the resulting compounds were studied by cyclic voltammetry and ESR spectroscopy. The three-dimensional structures were determined by the quantum-chemical PM3 and DFT/PBE/TZ2P methods.

引用

页码：334 / 341

页数：8

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