Heterogeneously Catalyzed Continuous-Flow Hydrogenation Using Segmented Flow in Capillary Columns

被引：43

作者：

Bakker, Jasper J. W. ^{[1
]}

Zieverink, Martijn M. P. ^{[1
]}

Reintjens, Raf W. E. G. ^{[2
]}

Kapteijn, Freek ^{[1
]}

Moulijn, Jacob A. ^{[1
]}

Kreutzer, Michiel T. ^{[1
]}

机构：

[1] Delft Univ Technol, Dept Chem Engn, NL-2628 BL Delft, Netherlands

[2] DSM Pharmaceut Prod ASC&D, NL-6160 MD Geleen, Netherlands

来源：

CHEMCATCHEM | 2011年 / 3卷 / 07期

关键词：

azides; flow reactions; heterogeneous catalysis; palladium; pharmaceutical intermediates; GAS-LIQUID; ORGANIC-SYNTHESIS; MASS-TRANSFER; SELECTIVE HYDROGENATION; REACTOR; MICROREACTOR; MICRO; INTENSIFICATION; SYSTEMS; DEVICE;

D O I：

10.1002/cctc.201100044

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

[No abstract available]

引用

页码：1155 / 1157

页数：3

共 49 条

[11] Micro reactors: principles and applications in organic synthesis [J].

Fletcher, PDI ;

Haswell, SJ ;

Pombo-Villar, E ;

Warrington, BH ;

Watts, P ;

Wong, SYF ;

Zhang, XL .

TETRAHEDRON, 2002, 58 (24) :4735-4757

[12] Microreactors as tools for synthetic chemists -: The chemists' round-bottomed flask of the 21st century? [J].

Geyer, Karolin ;

Codee, Jeroen D. C. ;

Seeberger, Peter H. .

CHEMISTRY-A EUROPEAN JOURNAL, 2006, 12 (33) :8434-8442

[13]

Günther A, 2006, LAB CHIP, V6, P1487, DOI 10.1039/b609851g

[14] A Palladium Wall Coated Microcapillary Reactor for Use in Continuous Flow Transfer Hydrogenation [J].

Hornung, Christian H. ;

Hallmark, Bart ;

Mackley, Malcolm R. ;

Baxendale, Ian R. ;

Ley, Steven V. .

ADVANCED SYNTHESIS & CATALYSIS, 2010, 352 (10) :1736-1745

[15] Chemistry in microstructured reactors [J].

Jähnisch, K ;

Hessel, V ;

Löwe, H ;

Baerns, M .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2004, 43 (04) :406-446

[16]

Jahnisch K., 2004, Angewandte Chemie, V116, P410, DOI DOI 10.1002/ANGE.200300577

[17] Microfluidic synthesis of colloidal silica [J].

Khan, SA ;

Günther, A ;

Schmidt, MA ;

Jensen, KF .

LANGMUIR, 2004, 20 (20) :8604-8611

[18] Combining enabling techniques in organic synthesis: Continuous flow processes with heterogenized catalysts [J].

Kirschning, Andreas ;

Solodenko, Wladimir ;

Mennecke, Klaas .

CHEMISTRY-A EUROPEAN JOURNAL, 2006, 12 (23) :5972-5990

[19] A microfluidic device for conducting gas-liquid-solid hydrogenation reactions [J].

Kobayashi, J ;

Mori, Y ;

Okamoto, K ;

Akiyama, R ;

Ueno, M ;

Kitamori, T ;

Kobayashi, S .

SCIENCE, 2004, 304 (5675) :1305-1308

[20] Sample dispersion for segmented flow in microchannels with rectangular cross section [J].

Kreutzer, Michiel T. ;

Gunther, Axel ;

Jensen, Klavs F. .

ANALYTICAL CHEMISTRY, 2008, 80 (05) :1558-1567

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