Synthesis of New Heterocyclic System of 4,5,7,8-Tetrahydroimidazo[1,2-c][1,3] thiazolo [4,5-e][1,3,2] diazaphosphinine Starting from 2-Aroylamino-3,3-dichloroacrylonitrile

被引：9

作者：

Kozachenko, Alexander P. ^{[1
]}

Shablykin, Oleg V. ^{[1
]}

Gakh, Andrei A. ^{[2
]}

Rusanov, Eduard B. ^{[3
]}

Brovarets, Vladimir S. ^{[1
]}

机构：

[1] Natl Acad Sci Ukraine, Inst Bioorgan Chem & Petrochem, Kiev, Ukraine

[2] Oak Ridge Natl Lab, Oak Ridge, TN 37831 USA

[3] Natl Acad Sci Ukraine, Inst Organ Chem, Kiev, Ukraine

来源：

HETEROATOM CHEMISTRY | 2010年 / 21卷 / 07期

关键词：

DERIVATIVES; NITRILES; AMINES;

D O I：

10.1002/hc.20638

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Easily accessible 2-aroylamino-3,3-dichloroacrylonitriles, when treated successively with ethylenediamine, phosphorus pentasulfide, water, and methyl and benzyl halides, furnish the corresponding derivatives of 4,5,7,8-tetrahydroimidazo[1,2-c] [1,3] thiazolo[4,5-e][1,3,2] diazaphosphinine, a novel-fused heterocycle. The structure of the compounds obtained is unequivocally confirmed by the spectroscopic method and X-ray diffraction analysis. (C) 2010 Wiley Periodicals, Inc. Heteroatom Chem 21:492-498, 2010; View this article online at wileyonlinelibrary.com. DOI 10.1002/hc.20638

引用

页码：492 / 498

页数：7

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