Aqueous-Mediated green synthesis of novel spiro[indole-quinazoline] derivatives using kit-6 mesoporous silica coated Fe3O4 nanoparticles as catalyst

被引：38

作者：

Abdolmohammadi, Shahrzad ^{[1
]}

Shariati, Shahab ^{[2
]}

Fard, Narges Elmi ^{[3
]}

Samani, Amir ^{[1
]}

机构：

[1] Islamic Azad Univ, Dept Chem, East Tehran Branch, POB 18735-138, Tehran, Iran

[2] Islamic Azad Univ, Dept Chem, Rasht Branch, Rasht, Iran

[3] Islamic Azad Univ, Young Researchers & Elite Club, South Tehran Branch, Tehran, Iran

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2020年 / 57卷 / 07期

关键词：

IN-VITRO; ARYLMETHYLIDENEPYRUVIC ACIDS; CYCLOCONDENSATION REACTION; MAGNETITE NANOPARTICLES; TIO2; NANOPARTICLES; HIGHLY EFFICIENT; MILD SYNTHESIS; NANOCOMPOSITE; ANTICANCER; ROUTE;

D O I：

10.1002/jhet.3981

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

In this work, a series of eight new spiro[3,4 ']1,3-dihydro-2H-indol-2-one-2 '-amino-4 ',6 ',7 ',8 '-tetrahydro-2 ',5'(1'H,3'H)-quinazoline-diones were successfully synthesized through a three-component reaction of 1H-indole-2,3-diones (isatins), guanidine nitrate, and 1,3-cyclohexanediones, by use of Kit-6 mesoporous silica coated Fe3O4 nanoparticles (Fe3O4@SiO2@KIT-6) as a highly efficient magnetically separable nanocatalyst in aqueous media at 60 degrees C. Several notable features of thiseco-friendly protocol are high yields of products, short reaction times, operational simplicity, and the use of easily available and recyclable catalyst.

引用

页码：2729 / 2737

页数：9

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