Studies of an Intermolecular Hydrogen-Bonded Complex of Butyloxy Benzoic Acid and Dipyridyl Ethylene

被引：3
|
作者：
Sambyal, Ambika [1 ]
Kour, Gurpreet [1 ]
Sharma, Shivangi [1 ]
Bamezai, Rajinder K. [1 ]
Anthal, Sumati [2 ]
Gupta, Vivek K. [2 ]
Kant, Rajni [2 ]
Yelamaggad, C. V. [3 ]
机构：
[1] Univ Jammu, Dept Chem, Jammu 180006, India
[2] Univ Jammu, Dept Phys, Jammu 180006, India
[3] Ctr Soft Matter Res, Jalahalli Bangalore, Bengaluru, India
来源：
MOLECULAR CRYSTALS AND LIQUID CRYSTALS | 2015年 / 608卷 / 01期
关键词：
phase transition; p-n-alkoxy benzoic acid; smectic A phase; Hydrogen bonding; STABILIZATION;
D O I：
10.1080/15421406.2014.953745
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A symmetric hydrogen-bonded liquid crystalline complex was synthesized from 4-n-butyloxy benzoic acid and 1,2-di-(4-pyridyl)-ethylene. The complex was analyzed by optical polarizing microscopy, differential scanning calorimetery, and thermal gravimetric analysis. The existence of hydrogen-bonding for the complex was confirmed by Fourier transform infrared spectroscopy and x-ray crystallography. The liquid crystalline complex crystallizes with a triclinic space group P1with the parameters a = 7.3331(4) angstrom, b = 9.0701(4) angstrom, c = 11.6957(5) angstrom and alpha = 81.896(4)degrees, beta = 79.239(4)degrees, and gamma = 85.652(4)degrees.
引用
收藏
页码：135 / 145
页数：11
相关论文
共 50 条
  • [21] PROTON POTENTIAL IN COMPLEX HYDROGEN-BONDED CATIONS
    WOOD, JL
    JOURNAL OF MOLECULAR STRUCTURE, 1973, 17 (02) : 307 - 328
  • [22] The model dipole moment of a hydrogen-bonded complex
    Melikova, SM
    Shchepkin, DN
    OPTICS AND SPECTROSCOPY, 1998, 84 (02) : 172 - 177
  • [23] ABINITIO MO STUDY OF HYDROGEN-BONDED COMPLEX - NORADRENALINE - FORMIC-ACID
    HODOSCEK, M
    KOCJAN, D
    SOLMAJER, T
    CROATICA CHEMICA ACTA, 1984, 57 (01) : 65 - 74
  • [24] CONCENTRATION AND SOLVENT EFFECTS ON THE HYDROGEN-BONDED COMPLEX OF QUINOLINE WITH TRIFLUOROACETIC-ACID
    DEGASZAFRAN, Z
    DULEWICZ, E
    SZAFRAN, M
    JOURNAL OF MOLECULAR LIQUIDS, 1991, 48 (2-4) : 335 - 346
  • [25] Structure and properties of a ferrocenylpyrimidine-bromanilic acid hydrogen-bonded supramolecular complex
    Mochida, Tomoyuki
    INORGANICA CHIMICA ACTA, 2010, 363 (13) : 3624 - 3626
  • [26] Microwave spectroscopic and ab initio studies of the hydrogen-bonded trimethylamine-hydrogen sulfide complex
    Tubergen, MJ
    Flad, JE
    DelBene, JE
    JOURNAL OF CHEMICAL PHYSICS, 1997, 107 (07): : 2227 - 2231
  • [27] Formation and reduction of hydrogen-bonded graphene oxide-poly(ethylene oxide) complex fiber
    Li, Jiefu
    Huang, Wentao
    Liu, Dezhong
    Sun, Jiaxing
    Zhu, Liping
    Wang, Yi
    Yang, Shuguang
    MATERIALS TODAY COMMUNICATIONS, 2019, 19 : 425 - 432
  • [28] Intermolecular Coulombic Decay in Small Biochemically Relevant Hydrogen-Bonded Systems
    Stoychev, Spas D.
    Kuleff, Alexander I.
    Cederbaum, Lorenz S.
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2011, 133 (17) : 6817 - 6824
  • [29] Intermolecular dissociation energies of hydrogen-bonded 1-naphthol complexes
    Knochenmuss, Richard
    Sinha, Rajeev K.
    Poblotzki, Anja
    Den, Takuya
    Leutwyler, Samuel
    JOURNAL OF CHEMICAL PHYSICS, 2018, 149 (20):
  • [30] THEORETICAL-STUDIES OF THE HYDROGEN-BONDED AND LITHIUM BONDED COMPLEXES
    LATAJKA, Z
    SCHEINER, S
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1984, 187 (APR): : 95 - PHYS
12345