Bi3+ and V3+ co-substituted Ni-Co spinel ferrites: Synthesis, optical, magnetic characterization and hyperfine interaction

被引：17

作者：

Almessiere, Munirah A. ^{[1
,2
]}

Slimani, Yassine ^{[1
]}

Gungunes, Hakan ^{[3
]}

Gondal, Mohammed A. ^{[4
,5
]}

Hassan, M. ^{[6
]}

Shirsath, Sagar E. ^{[7
]}

Baykal, Abdulhadi ^{[8
]}

机构：

[1] Imam Abdulrahman Bin Faisal Univ, Inst Res & Med Consultat IRMC, Dept Biophys, POB 1982, Dammam 31441, Saudi Arabia

[2] Imam Abdulrahman Bin Faisal Univ, Coll Sci, Dept Phys, POB 1982, Dammam 31441, Saudi Arabia

[3] Hitit Univ, Dept Phys, Cevre Yolu Bulvari, TR-19030 Corum, Turkey

[4] King Fahd Univ Petr & Minerals, Phys Dept, Laser Res Grp, IRC Hydrogen & Energy Storage, Dhahran 31261, Saudi Arabia

[5] King Fahd Univ Petr & Minerals, KA CARE Energy Res & Innovat Ctr, Dhahran 31261, Saudi Arabia

[6] King Fahd Univ Petr & Minerals KFUPM, Phys Dept, Laser Res Grp, Dhahran 31261, Saudi Arabia

[7] Univ New South Wales, Sch Mat Sci & Engn, Sydney, NSW 2052, Australia

[8] Imam Abdulrahman Bin Faisal Univ, Inst Res & Med Consultat IRMC, Dept Nanomed Res, POB 1982, Dammam 31441, Saudi Arabia

来源：

MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS | 2022年 / 284卷

关键词：

Ni-Co spinel nanoferrites; Bi3+-V3+ ions co-substitution; Mossbauer analysis; XPS study; Magnetic features; NEUTRON-DIFFRACTION; CATION DISTRIBUTION; NANOPARTICLES;

D O I：

10.1016/j.mseb.2022.115905

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Ni0.5Co0.5VxBixFe2-2xO4 spinel ferrite nanoparticles with composition (x = 0.00, 0.02, 0.04, 0.06 and 0.08) (CoNiVBiFeO (x = 0.00-0.08) SFNPs) were well fabricated hydrothermally. The consequence of co-substitution of both Bi3+ and V3+ ions on structure, morphology, and magnetic features of Ni0.5Co0.5Fe2O4 SFNPs were studied using XRD (X-ray diffractometry), scanning (SEM) and transmission (TEM) electron microscopies along with EDX, XPS (X-ray photoelectron spectroscopy), VSM (vibrating sample magnetometry) and Mossbauer spectroscopic techniques. The pure spinel ferrite (SFs) phase was approved via XRD. The morphology of SFNPs were revealed by SEM and TEM. Hyperfine parameters are determined from fitting room temperature Mossbauer spectra. The V3+ and Bi3+ ions occupy mainly at B site. The isomer shift values are coupled with the characteristics of the high spin Fe3+ ion. The influence of V3+ and Bi3+ ions co-doping on the magnetic features of Ni-Co SFNPs has been also investigated at 300 and 10 K. The saturation magnetization (M-s), remanence (M-r), coercive field (H-c), and Bohr magneton number (n(B)) are extracted from the recorded M-H hysteresis loops. Nanomagnetic materials with x content of 0.02, 0.08, and 0.10 exhibited superparamagnetic (SPM) behavior, whereas other products with x content of 0.00, 0.04, and 0.06 displayed soft ferrimagnetic behavior at ambient temperature. The different prepared nanoferrites displayed hard ferrimagnetic characteristic at 10 K. The M-s and M-r values are decreased as result of V3+ and Bi3+ ions co-doping. However, H-c does not show a monotonic trend. The fluctuations in magnetic moments of ions, super-exchange coupling, and distribution of cations are correlated with the changes in magnetic parameters to explain their variations.

引用

页数：11

共 60 条

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