Structural Phase Stability, Morphological and Magnetic Characterization of a New Orthorhombic Spinel (MgZn2O4) Nano-Particle Prepared via Citrate-Gel Auto Combustion Method

被引：0
作者：
Singh, Alok Kumar [1 ]
Dhillon, Anju [2 ]
Senguttuvan, T. D. [3 ]
Siddiqui, Azher M. [1 ]
机构：
[1] Jamia Millia Islamia, Dept Phys, New Delhi 25, India
[2] GGSIP Univ, Maharaja Surajmal Inst Technol, Dept Appl Sci, New Delhi 58, India
[3] Natl Phys Lab, New Delhi 110012, India
来源：
ADVANCED SCIENCE LETTERS | 2014年 / 20卷 / 7-9期
关键词：
XRD; Spinel; SEM; EDAX; Superparamagnetic; Magnetic Susceptibility; CO;
D O I：
10.1166/asl.2014.5507
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
The study of structural phase stability, morphological and magnetic properties of orthorhombic spinel (MgZn2O4) synthesized through citrate-gel auto combustion method has been taken away. The samples were characterized by using XRD, SEM and energy dispersive X-ray (EDAX) and magnetic susceptibility. These spinel compounds have been synthesized for the first time to the best of our knowledge. XRD studies confirm the single phase orthorhombic spinel structure of the sample. The crystallite size was found to be of 64.76 nm by Debye Scherrer formula of MgZn2O4 spinel compounds. The values of lattice parameters a, b and c have been calculated by powder-X software. The compositional formation was confirmed by EDAX. SEM micrograph shows spherical shape with nano-crystalline behaviour. The Magnetic susceptibility graph shows the superparamagnetic behaviour of the compound.
引用
收藏
页码：1662 / 1665
页数：4
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