Raman diagnostics of multi-wall carbon nanotubes with a small wall number

被引:40
作者
Bokova, S. N. [1 ]
Obraztsova, E. D. [1 ]
Grebenyukov, V. V. [1 ]
Elumeeva, K. V. [2 ,3 ,4 ]
Ishchenko, A. V. [2 ,4 ]
Kuznetsov, V. L. [2 ,4 ,5 ]
机构
[1] RAS, AM Prokhorov Gen Phys Inst, Moscow 119991, Russia
[2] SB RAS, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
[3] SB RAS, Nikolaev Inst Inorgan Chem, Novosibirsk 630090, Russia
[4] Novosibirsk State Univ, Novosibirsk 630090, Russia
[5] Novosibirsk State Tech Univ, Novosibirsk 630092, Russia
来源
PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS | 2010年 / 247卷 / 11-12期
关键词
multi-wall carbon nanotubes; Raman scattering;
D O I
10.1002/pssb.201000237
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Raman spectroscopy study of multi-wall carbon nanotubes (MWNTs) of different diameters (with a small controllable number of walls) produced using Fe-Co catalyst with a variable size of the same active component has been performed. We have characterized as produced MWNTs with different diameters (series 1) and two types of tubes with fixed mean diameters (similar to 10 and 20 nm) heated in a flow of pure argon at various temperatures (2200, 2600, and 2800 degrees C-series 2). The Raman spectra of MWNTs have been registered in three spectral regions, corresponding to D (disorder-induced), G (graphite) and 2D (two-phonon scattering) bands. A ratio of intensities I(2D)/I(D) of tubes of series 1 has demonstrated almost a linear dependence on the nanotube diameters. After heating (series 2), D (disorder-induced) Raman band has shown a substantial decrease in intensity. The variation of the Raman spectra parameters is discussed in terms of defectiveness of nanotubes. (c) 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
引用
收藏
页码:2827 / 2830
页数:4
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