Synthesis and Characterization of Novel Titanium Dioxide Microspheres with Exposed {001} Facets

被引:4
作者
Luo, Zhi-Hui [1 ]
Zhou, Xiao-Song [2 ,3 ]
Jin, Bei [2 ,3 ]
Luo, Jin [2 ,3 ]
Xu, Xu-Yao [2 ,3 ]
Chen, Liu-Yong [2 ,3 ]
机构
[1] Yulin Normal Univ, Coll Chem & Mat, Yulin 537000, Peoples R China
[2] Lingnan Normal Univ, Sch Chem & Chem Engn, Zhanjiang 524048, Peoples R China
[3] Lingnan Normal Univ, Inst Phys Chem, Zhanjiang 524048, Peoples R China
关键词
ANATASE TIO2; PHOTOCATALYTIC ACTIVITY; NANOPARTICLES; NANOCRYSTALS; NANOSHEETS; PERCENTAGE;
D O I
10.1246/cl.141051
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Novel anatase titanium dioxide (TiO2) microspheres with exposed 0011 facets were successfully synthesized via a facile and controllable hydrothermal approach using sodium fluoroborate as the reagent. The products were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). XRD results showed that the TiO2 microspheres were anatase phase and had good crystallinity. SEM images showed that the as-prepared TiO2 samples displayed surface of microspheres with exposed 0011 facets and a mean diameter of 3.2 mu m Experimental results revealed that the as-prepared TiO2 microspheres might be assembled by nanosheets. The formation process of the TiO2 microspheres was preliminarily investigated.
引用
收藏
页码:256 / 258
页数:3
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