Automated preparation of high-quality epitaxial graphene on 6H-SiC(0001)

被引:67
作者
Ostler, Markus [1 ]
Speck, Florian [1 ]
Gick, Markus [1 ]
Seyller, Thomas [1 ]
机构
[1] Univ Erlangen Nurnberg, Lehrstuhl Tech Phys, D-91058 Erlangen, Germany
来源
PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS | 2010年 / 247卷 / 11-12期
关键词
graphene; SiC; growth; XPS; AFM; SILICON-CARBIDE; BERRYS PHASE; GRAPHITE; LAYERS; GAS;
D O I
10.1002/pssb.201000220
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
In this contribution, we present details on a recently installed hot-wall reactor for graphene growth on silicon carbide (SiC) in argon under atmospheric pressure. Both preparation steps, i.e., the preconditioning of the SiC substrate by hydrogen etching and the graphene growth are performed in this setup in a fully automated manner thus ensuring the preparation of high-quality graphene on an everyday basis. Samples were characterized by atomic force microscopy and X-ray induced photoelectron spectroscopy. We present results on the optimization of the hydrogen etching procedure. The thickness distribution of graphene samples grown in the automated process is Gaussian with a mean value of 1.1 monolayers and a standard deviation of 0.17 monolayers. This indicates a highly controlled process. (C) 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
引用
收藏
页码:2924 / 2926
页数:3
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