Pectin as a natural biopolymer catalyst promoted green synthesis of dihydropyrano[2,3-c]pyrazole derivatives in aqueous ethanol media

被引:0
作者
Mohamadpour, Farzaneh [1 ]
机构
[1] Apadana Inst Higher Educ, Sch Engn, Shiraz, Iran
来源
INDIAN JOURNAL OF CHEMISTRY | 2022年 / 61卷 / 04期
关键词
Pectin; natural biopolymer catalyst; dihydropyrano[2,3-c]pyrazoles; green protocol; aqueous ethanol media; four-component condensation; ONE-POT SYNTHESIS; MULTICOMPONENT SYNTHESIS; ECO-SAFE; BIODEGRADABLE CATALYST; 4-COMPONENT SYNTHESIS; BIOLOGICAL-ACTIVITY; CONVENIENT; ACID; EFFICIENT; CAFFEINE;
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A green and one-pot protocol for the facile synthesis of biologically important dihydropyrano[2,3-c]pyrazole derivatives has been developed. In this method pectin has been utilized as a natural biopolymer catalyst to get quick access to the dihydropyrano[2,3-c]pyrazole derivatives in aqueous ethanol media and short reaction times. The main advantages of this method are the operational simplicity, reduced reaction time, high yield of the products, avoidance of any hazardous organic solvent, toxic catalyst, tedious purification step, convenient work up procedure and employment of natural, highly efficient and readily available catalyst. All these factors make the present method economical, green and sustainable.
引用
收藏
页码:405 / 410
页数:6
相关论文
共 50 条
  • [1] Melamine, a Recyclable Catalyst for the Synthesis of Dihydropyrano[2,3-c]pyrazoles in Aqueous Ethanol
    Mohamadpour, Farzaneh
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2024, 56 (02) : 163 - 168
  • [2] Natural Phosphate K09 as a New Reusable Catalyst for the Synthesis of Dihydropyrano[2,3-c]Pyrazole Derivatives at Room Temperature
    El Mejdoubi, K.
    Sallek, B.
    Digua, K.
    Chaair, H.
    Oudadesse, H.
    KINETICS AND CATALYSIS, 2019, 60 (04) : 536 - 542
  • [3] β-Cyclodextrin as a supramolecular catalyst for the synthesis of dihydropyrano[2,3-c]pyrazole and spiro[indoline-3,4′-pyrano [2,3-c]pyrazole] in aqueous medium
    Tayade, Yogesh A.
    Padvi, Swapnil A.
    Wagh, Yogesh B.
    Dalai, Dipak S.
    TETRAHEDRON LETTERS, 2015, 56 (19) : 2441 - 2447
  • [4] DABCO catalyzed rapid one-pot synthesis of 1,4-dihydropyrano [2,3-c] pyrazole derivatives in aqueous media
    Waghmare, Amit S.
    Pandit, Shivaji S.
    JOURNAL OF SAUDI CHEMICAL SOCIETY, 2017, 21 (03) : 286 - 290
  • [5] Bovine serum albumin catalyzed one-pot, three-component synthesis of dihydropyrano[2,3-c] pyrazole derivatives in aqueous ethanol
    Dalal, Kiran S.
    Tayade, Yogesh A.
    Wagh, Yogesh B.
    Trivedi, Darshak R.
    Dalal, Dipak S.
    Chaudhari, Bhushan L.
    RSC ADVANCES, 2016, 6 (18): : 14868 - 14879
  • [6] SODIUM GLUCONATE: AN EFFICIENT ORGANOCATALYST FOR THE SYNTHESIS OF DIHYDROPYRANO[2,3-C]PYRAZOLE DERIVATIVES
    Khandebharad, Amol
    Sarda, Swapnil
    Soni, Mahesh
    Agrawal, Brijmohan
    BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA, 2019, 33 (02) : 331 - 340
  • [7] Caffeine as a Naturally Green and Biodegradable Catalyst for Preparation of Dihydropyrano[2,3-c]pyrazoles
    Mohamadpour, Farzaneh
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2020, 52 (05) : 453 - 457
  • [8] Novel 1,4-dihydropyrano[2,3-c]pyrazole derivatives: Synthesis, characterization, biological evaluation and in silico study
    Vasava, Mahesh S.
    Bhoi, Manoj N.
    Rathwa, Sanjay K.
    Shetty, Shilpa S.
    Patel, Rikin D.
    Rajani, Dhanji P.
    Rajani, Smita D.
    Patel, Alpesh
    Pandya, Himanshu A.
    Patel, Hitesh D.
    JOURNAL OF MOLECULAR STRUCTURE, 2019, 1181 : 383 - 402
  • [9] Natural Phosphate K09 as a New Reusable Catalyst for the Synthesis of Dihydropyrano[2,3-c]Pyrazole Derivatives at Room Temperature
    K. El Mejdoubi
    B. Sallek
    K. Digua
    H. Chaair
    H. Oudadesse
    Kinetics and Catalysis, 2019, 60 : 536 - 542
  • [10] AN EFFICIENT AND GREEN PROTOCOL FOR THE SYNTHESIS OF DIHYDROPYRANO [2,3-C] PYRAZOLES IN AQUEOUS MEDIUM USING THIAMINE HYDROCHLORIDE AS A CATALYST
    Nikam, Mukesh D.
    Mahajan, Pravin S.
    Chate, Asha V.
    Dabhade, Sanjay K.
    Gill, Charansingh H.
    JOURNAL OF THE CHILEAN CHEMICAL SOCIETY, 2015, 60 (01): : 2847 - 2850