Fabrication of novel green magnetic electrospun nanofibers based on Fe3O4 nanoparticles/PVA/chitosan/collagen

被引:13
作者
Abou-okeil, A. [1 ]
Refaie, R. [1 ]
Khalil, E. M. [2 ]
Mostafa, Sh E. [1 ]
Ibrahim, Hassan M. [1 ]
机构
[1] Natl Res Ctr, Pretreatment & Finishing Cellulos Fibers Dept, Text Ind Res Div, 33 El Bohouth St,PO 12622, Cairo, Egypt
[2] Helwan Univ, Fac Sci, Chem Dept, Helwan, Egypt
来源
EGYPTIAN JOURNAL OF CHEMISTRY | 2022年 / 65卷 / 08期
关键词
novel green; magnetic electrospun nanofibers; Fe3O4; nanoparticles; polyvinyl alcohol; chitosan; collagen; POLYESTER FABRICS; GRAPHENE OXIDE; NANOPARTICLES; DRUG; CHITOSAN; COTTON; DELIVERY; NANOCOMPOSITE; CELLULOSE; ACID;
D O I
10.21608/ejchem.2022.109235.4980
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Herein iron oxide nanoparticles were successfully prepared from FeCl3 center dot 6H(2)O (1.1 g) and FeCl2 center dot 4H(2)O (0.4 g) by addition of ammonium hydroxide via coprecipitation method (CPC). The conditions for the preparation of IONPs were optimized IONPs were characterized by transmission electron microscope (TEM) and vibrating sample magnetometer (VSM). Magnetic electrospun nanofibers based on Fe3O4 nanoparticles/PVA/chitosan/collagen were fabricated using an electrospinning technique. In the absence and presence of ciprofloxacin, nanofibers were made from Fe3O4 nanoparticles that made up around 10% of the polymers. The viscosity and conductivity of several composite polymer formulations were measured as critical metrics. The electrospun nanofibers were characterized by Fourier transformation infrared spectroscopy (ATR- FTIR) and scanning electron microscope (SEM). The diameter of the nanofibers, antibacterial capabilities, and magnetism of the nanofibers were all measured. Electrospun magnetic nanofibers with higher antibacterial activity and supermagnetism were produced. In addition, the use of ciprofloxacin antibiotics improved these qualities.
引用
收藏
页码:283 / 299
页数:17
相关论文
共 68 条
[1]  
Abdel-Mohdy FA, 2016, EGYPT J CHEM, V59, P45
[2]   Hyaluronic Acid/Oxidized K-Carrageenan Electrospun Nanofibers Synthesis and Antibacterial Properties [J].
Abou-Okeil, A. ;
Fahmy, H. M. ;
Fouda, Moustafa M. G. ;
Aly, A. A. ;
Ibrahim, H. M. .
BIONANOSCIENCE, 2021, 11 (03) :687-695
[3]   Chitosan phosphate induced better thermal characteristics to cotton fabric [J].
Abou-Okeil, A. ;
El-Shafie, A. ;
Hebeish, A. .
JOURNAL OF APPLIED POLYMER SCIENCE, 2007, 103 (03) :2021-2026
[4]   Biocompatible hydrogel for cartilage repair with adjustable properties [J].
Abou-Okeil, Ashraf ;
Ahmed, Amal ;
Amr, Ahmed ;
Soliman, Ahmed Abdel-Fattah .
POLYMERS FOR ADVANCED TECHNOLOGIES, 2019, 30 (08) :2026-2033
[5]  
Ali M., 2021, Egyptian Journal of Chemistry
[6]   Synthesis of a novel biocompatible nanocomposite of graphene oxide and magnetic nanoparticles for drug delivery [J].
Aliabadi, Majid ;
Shagholani, Hamidreza ;
Lehi, Arash Yunessnia .
INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES, 2017, 98 :287-291
[7]   Grafting of N-vinyl-2-pyrrolidone onto κ-carrageenan for silver nanoparticles synthesis [J].
Aly, A. A. ;
Abou-Okeil, A. ;
Fahmy, H. M. .
CARBOHYDRATE POLYMERS, 2018, 198 :119-123
[8]   Preparation and Characterization of Polyethylene Glycol/Dimethyl Siloxane Adduct and Its Utilization as Finishing Agent for Cotton Fabric [J].
Aly, A. S. ;
Abdel-Mohsen, A. M. ;
Hrdina, R. ;
Abou-Okeil, A. .
JOURNAL OF NATURAL FIBERS, 2011, 8 (03) :176-188
[9]   Squalene Based Nanocomposites: A New Platform for the Design of Multifunctional Pharmaceutical Theragnostics [J].
Arias, Jose L. ;
Reddy, L. Harivardhan ;
Othman, Mohammad ;
Gillet, Brigitte ;
Desmaele, Didier ;
Zouhiri, Fatima ;
Dosio, Franco ;
Gref, Ruxandra ;
Couvreur, Patrick .
ACS NANO, 2011, 5 (02) :1513-1521
[10]   Covalent immobilization of trypsin onto modified magnetite nanoparticles and its application for casein digestion [J].
Atacan, Keziban ;
Cakiroglu, Bekir ;
Ozacar, Mahmut .
INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES, 2017, 97 :148-155