Synthesis, structure and characterization of some Schiff bases bearing phenylferrocene

被引：7
|
作者：
Shah, Faiz Ullah
Akhter, Zareen [1 ]
Siddiqi, Humaira M.
Parvez, Masood
机构：
[1] Quaid I Azam Univ, Dept Chem, Islamabad 45320, Pakistan
[2] Univ Calgary, Dept Chem, Calgary, AB T2N 1N4, Canada
来源：
APPLIED ORGANOMETALLIC CHEMISTRY | 2007年 / 21卷 / 09期
关键词：
ferrocene; Schiff bases; phenylferrocene;
D O I：
10.1002/aoc.1255
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Some novel Schiff bases bearing phenylferrocene were synthesized by condensation reaction of 4-ferrocenylaniline with different aromatic aldehydes. The compounds prepared were characterized by spectroscopic methods (IR, UV-visible, H-1 and C-13 NMR) and elemental analysis. The single crystal analysis of compound F1 [monoclinic, space group, P2(1)/c (no. 14), a = 1.9.858(2), b = 7.416(2), c = 12.095(5) angstrom, beta = 106.257(14)degrees] indicates a trans imine bond with a bond length of 1.270(2) angstrom, typical of a carbon-nitrogen double bond. Copyright (c) 2007 John Wiley & Sons, Ltd.
引用
收藏
页码：758 / 762
页数：5
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