Revealing Three-Dimensional Structure of an Individual Colloidal Crystal Grain by Coherent X-Ray Diffractive Imaging

被引：27

作者：

Shabalin, A. G. ^{[1
,2
]}

Meijer, J. -M. ^{[3
]}

Dronyak, R. ^{[1
]}

Yefanov, O. M. ^{[1
]}

Singer, A. ^{[1
]}

Kurta, R. P. ^{[1
]}

Lorenz, U. ^{[1
]}

Gorobtsov, O. Y. ^{[1
,4
]}

Dzhigaev, D. ^{[1
,5
]}

Kalbfleisch, S. ^{[6
]}

Gulden, J. ^{[1
]}

Zozulya, A. V. ^{[1
]}

Sprung, M. ^{[1
]}

Petukhov, A. V. ^{[3
,7
]}

Vartanyants, I. A. ^{[1
,5
]}

机构：

[1] Deutsch Elektronen Synchrotron DESY, Notkestr 85, D-22607 Hamburg, Germany

[2] RAS, AV Shubnikov Inst Crystallog, Leninskii Pr 59, Moscow 119333, Russia

[3] Univ Utrecht, Vant Hoff Lab Phys & Colloid Chem, Debye Inst Nanomat Sci, Padualaan 8, NL-3508 TB Utrecht, Netherlands

[4] NRC Kurchatov Inst, Pl Akad Kurchatova, Moscow 123182, Russia

[5] Natl Res Nucl Univ, MEPhI Moscow Engn Phys Inst, Kashirskoe Shosse 31, Moscow 115409, Russia

[6] Inst Xray Phys, Friedrich Hund Pl 1, D-37077 Gottingen, Germany

[7] Eindhoven Univ Technol, Lab Phys Chem, Dept Chem Engn & Chem, POB 513, NL-5600 MB Eindhoven, Netherlands

来源：

PHYSICAL REVIEW LETTERS | 2016年 / 117卷 / 13期

关键词：

HARD-SPHERE; ATOMIC-RESOLUTION; PHOTONIC-CRYSTALS; MICROSCOPY; SCATTERING; PARTICLES; DEFECTS; SYSTEM;

D O I：

10.1103/PhysRevLett.117.138002

中图分类号：

O4 [物理学];

学科分类号：

0702 ;

摘要：

We present results of a coherent x-ray diffractive imaging experiment performed on a single colloidal crystal grain. The full three-dimensional (3D) reciprocal space map measured by an azimuthal rotational scan contained several orders of Bragg reflections together with the coherent interference signal between them. Applying the iterative phase retrieval approach, the 3D structure of the crystal grain was reconstructed and positions of individual colloidal particles were resolved. As a result, an exact stacking sequence of hexagonal close-packed layers including planar and linear defects were identified.

引用

页数：6

共 61 条

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