Quantifying the dielectric constant of thick insulators using electrostatic force microscopy

被引:82
作者
Fumagalli, L. [1 ,2 ]
Gramse, G. [1 ,2 ]
Esteban-Ferrer, D. [1 ]
Edwards, M. A. [1 ]
Gomila, G. [1 ,2 ]
机构
[1] IBEC, Nanobioelec Grp, Barcelona 08028, Spain
[2] Univ Barcelona, Dept Elect, E-08028 Barcelona, Spain
关键词
borosilicate glasses; finite element analysis; insulating thin films; mica; nanostructured materials; permittivity; polymers; scanning probe microscopy; POLARIZATION;
D O I
10.1063/1.3427362
中图分类号
O59 [应用物理学];
学科分类号
摘要
Quantitative measurement of the low-frequency dielectric constants of thick insulators at the nanoscale is demonstrated utilizing ac electrostatic force microscopy combined with finite-element calculations based on a truncated cone with hemispherical apex probe geometry. The method is validated on muscovite mica, borosilicate glass, poly (ethylene naphthalate), and poly(methyl methacrylate). The dielectric constants obtained are essentially given by a nanometric volume located at the dielectric-air interface below the tip, independently of the substrate thickness, provided this is on the hundred micrometer-length scale, or larger. (C) 2010 American Institute of Physics. [doi: 10.1063/1.3427362]
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页数:3
相关论文
共 15 条
[1]   Local dielectric spectroscopy of polymer films [J].
Crider, P. S. ;
Majewski, M. R. ;
Zhang, Jingyun ;
Oukris, H. ;
Israeloff, N. E. .
APPLIED PHYSICS LETTERS, 2007, 91 (01)
[2]   Quantitative Nanoscale Dielectric Microscopy of Single-Layer Supported Biomembranes [J].
Fumagalli, Laura ;
Ferrari, Giorgio ;
Sampietro, Marco ;
Gomila, Gabriel .
NANO LETTERS, 2009, 9 (04) :1604-1608
[3]   Dielectric-constant measurement of thin insulating films at low frequency by nanoscale capacitance microscopy [J].
Fumagalli, Laura ;
Ferrari, Giorgio ;
Sampietro, Marco ;
Gomila, Gabriel .
APPLIED PHYSICS LETTERS, 2007, 91 (24)
[4]   High spatial resolution quantitative microwave impedance microscopy by a scanning tip microwave near-field microscope [J].
Gao, C ;
Wei, T ;
Duewer, F ;
Lu, YL ;
Xiang, XD .
APPLIED PHYSICS LETTERS, 1997, 71 (13) :1872-1874
[5]   Quantitative dielectric constant measurement of thin films by DC electrostatic force microscopy [J].
Gramse, G. ;
Casuso, I. ;
Toset, J. ;
Fumagalli, L. ;
Gomila, G. .
NANOTECHNOLOGY, 2009, 20 (39)
[6]   Obtaining the dielectric constant of solids from capacitance measurements with a pointer electrode [J].
Guadarrama-Santana, A. ;
Garcia-Valenzuela, A. .
REVIEW OF SCIENTIFIC INSTRUMENTS, 2009, 80 (10)
[7]   SCANNING POLARIZATION FORCE MICROSCOPY - A TECHNIQUE FOR IMAGING LIQUIDS AND WEAKLY ADSORBED LAYERS [J].
HU, J ;
XIAO, XD ;
SALMERON, M .
APPLIED PHYSICS LETTERS, 1995, 67 (04) :476-478
[8]   Quantitative analysis of dielectric constants from EFM images of multicomponent polymer blends [J].
Krayev, AV ;
Shandryuk, GA ;
Grigorov, LN ;
Talroze, RV .
MACROMOLECULAR CHEMISTRY AND PHYSICS, 2006, 207 (11) :966-969
[9]   Calibration of shielded microwave probes using bulk dielectrics [J].
Lai, K. ;
Kundhikanjana, W. ;
Kelly, M. A. ;
Shen, Z. X. .
APPLIED PHYSICS LETTERS, 2008, 93 (12)
[10]   Near-static dielectric polarization of individual carbon nanotubes [J].
Lu, Wei ;
Wang, Dan ;
Chen, Liwei .
NANO LETTERS, 2007, 7 (09) :2729-2733