Biodiesel Production from the Lipid of Wastewater Sludge Using an Acidic Heterogeneous Catalyst

被引:24
作者
Siddiquee, Muhammad N. [1 ]
Kazemian, Hossein [1 ]
Rohani, Sohrab [1 ]
机构
[1] Univ Western Ontario, Dept Chem & Biochem Engn, London, ON N6A 5B9, Canada
基金
加拿大自然科学与工程研究理事会;
关键词
Biodiesel; Fatty acid methyl ester; Lipid; Mesoporous heterogeneous catalyst; Wastewater sludge; SEWAGE-SLUDGE; TRANSESTERIFICATION; OILS; EXTRACTION; METHANOL;
D O I
10.1002/ceat.201100119
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The production of biodiesel from the lipid of wastewater sludge was studied using SBA-15 impregnated with the heteropolyacid H3PO4.12WO3.xH2O (PW12) as a mesoporous heterogeneous catalyst. X-ray diffraction, Brunauer-Emmett-Teller surface area, thermalgravimetric analysis, and scanning electron microscopy were applied to characterize the prepared catalysts. Catalytic performances were evaluated in a microreactor setup under different experimental conditions. The biodiesel yield for a sample impregnated with 15?% PW12 was 30.14?wt-% at a temperature of 135?degrees C and a pressure of 135?psi for 3?h reaction time.
引用
收藏
页码:1983 / 1988
页数:6
相关论文
共 23 条
[11]  
Knothe G., 2005, The Biodiesel Handbook, V1st, P1
[12]   Transesterification of triacetin with methanol on solid acid and base catalysts [J].
López, DE ;
Goodwin, JG ;
Bruce, DA ;
Lotero, E .
APPLIED CATALYSIS A-GENERAL, 2005, 295 (02) :97-105
[13]   Biodiesel production by in situ transesterification of municipal primary and secondary sludges [J].
Mondala, Andro ;
Liang, Kaiwen ;
Toghiani, Hossein ;
Hernandez, Rafael ;
French, Todd .
BIORESOURCE TECHNOLOGY, 2009, 100 (03) :1203-1210
[14]   Efficient two-step synthesis of biodiesel from greases [J].
Ngo, Helen L. ;
Zafiropoulos, Nicholas A. ;
Foglia, Thomas A. ;
Samulski, Edward T. ;
Lin, Wenbin .
ENERGY & FUELS, 2008, 22 (01) :626-634
[15]   A multi-criteria approach to screening alternatives for converting sewage sludge to biodiesel [J].
Pokoo-Aikins, Grace ;
Heath, Aubrey ;
Mentzer, Ray A. ;
Mannan, M. Sam ;
Rogers, William J. ;
El-Halwagi, Mahmoud M. .
JOURNAL OF LOSS PREVENTION IN THE PROCESS INDUSTRIES, 2010, 23 (03) :412-420
[16]   Biodiesel from activated sludge through in situ transesterification [J].
Revellame, Emmanuel ;
Hernandez, Rafael ;
French, William ;
Holmes, William ;
Alley, Earl .
JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY, 2010, 85 (05) :614-620
[17]  
Siddiquee M. N., 2011, THESIS U W ONTARIO L
[18]   Lipid extraction and biodiesel production from municipal sewage sludges: A review [J].
Siddiquee, Muhammad N. ;
Rohani, Sohrab .
RENEWABLE & SUSTAINABLE ENERGY REVIEWS, 2011, 15 (02) :1067-1072
[19]   Sludge dewatering and stabilization in drying reed beds: Characterization of three full-scale systems in Catalonia, Spain [J].
Uggetti, Enrica ;
Llorens, Esther ;
Pedescoll, Anna ;
Ferrer, Ivet ;
Castellnou, Roger ;
Garcia, Joan .
BIORESOURCE TECHNOLOGY, 2009, 100 (17) :3882-3890
[20]   Ordered Mesoporous Silica Material SBA-15: A Broad-Spectrum Formulation Platform for Poorly Soluble Drugs [J].
Van Speybroeck, Michiel ;
Barillaro, Valery ;
Do Thi, Thao ;
Mellaerts, Randy ;
Martens, Johan ;
Van Humbeeck, Jan ;
Vermant, Jan ;
Annaert, Pieter ;
Van Den Mooter, Guy ;
Augustijns, Patrick .
JOURNAL OF PHARMACEUTICAL SCIENCES, 2009, 98 (08) :2648-2658