A novel two-dimensional cadmium polymeric aminonaphthalene sulfonate and its application in the synthesis of CdS materials

被引：8

作者：

Mi, Li-Wei ^{[1
]}

Han, Min-Le ^{[2
]}

Li, Da-Peng ^{[1
]}

Chen, Wei-Hua ^{[1
]}

Zheng, Zhi ^{[1
]}

机构：

[1] Xuchang Univ, Inst Surface Micro & Nano Mat, Xuchang, Peoples R China

[2] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang, Peoples R China

来源：

ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 2008年 / 634卷 / 02期

关键词：

cadmium; cadmium sulphide; cystal structure;

D O I：

10.1002/zaac.200700396

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new mixed-ligand complex, [CdL(bipy)(CH3OH)(NO3)](n) (1), (HL = 4-amino-1-naphthalene sulfonic acid and bipy = 4,4'-bipyridine) could be achieved by combining (d(10) Cd2+ to HL and bridging ligand 4,4'-bipy. The structure is characterized by X-ray single-crystal diffraction. 4-amino-1-naphthalene sulfonate and 4,4'-bipyridine act as bridging ligands, linking two adjacent Cd-II atom to form a two-dimensional coordination polymer, respectively N-H center dot center dot center dot O hydrogen-bonding interaction between these networks to form the face-to-face three-dimensional architecture. By carrying out the reaction of polymeric cadmium naphthalene sulfonate with Na2S in the presence of sodium hydroxide, scale-like CdS materials have been obtained. The structure has been characterized by scanning electron microscopy and powder X-ray diffraction.

引用

页码：373 / 376

页数：4

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