Microwave assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four pyridyl groups

被引：23

作者：

Biyiklioglu, Zekeriya ^{[1
]}

Kantekin, Halit ^{[1
]}

机构：

[1] Karadeniz Tech Univ, Dept Chem, TR-61080 Trabzon, Turkey

来源：

TRANSITION METAL CHEMISTRY | 2007年 / 32卷 / 07期

关键词：

D O I：

10.1007/s11243-007-0212-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The novel tetrasubstituted metal-free phthalocyanine (4) and metallophthalocyanines (5, 6, 7 and 8) bearing four pyridyl group moieties on peripheral positions have been synthesized by cyclotetramerization of the phthalonitrile derivative (3) in a multi-step reaction sequence. The new compounds were characterized by a combination of elemental analysis, H-1- and C-13-n.m.r., i.r., U.V.-vis and m.s. spectral data.

引用

页码：851 / 856

页数：6

共 54 条

[1]

ABDURRAHMANOGLU S, 2004, J CHEM DA, V4022

[2] DICOPPER(II) CHLORO AND AZIDO INCLUSION COMPLEXES OF THE [24-ANE-N2S4] BINUCLEATING MACROCYCLE - SYNTHESIS, CRYSTAL AND MOLECULAR-STRUCTURES, AND SPECTRAL, MAGNETIC, AND ELECTROCHEMICAL PROPERTIES [J].

AGNUS, Y ;

LOUIS, R ;

GISSELBRECHT, JP ;

WEISS, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1984, 106 (01) :93-102

[3]

[Anonymous], [No title captured]

[4] Nanocap-shaped tin phthalocyanines:: Synthesis, characterization, and corrosion inhibition activity [J].

Beltrán, HI ;

Esquivel, R ;

Lozada-Cassou, M ;

Dominguez-Aguilar, MA ;

Sosa-Sánchez, A ;

Sosa-Sánchez, JL ;

Höpfl, H ;

Barba, V ;

Luna-García, R ;

Farfán, N ;

Zamudio-Rivera, LS .

CHEMISTRY-A EUROPEAN JOURNAL, 2005, 11 (09) :2705-2715

[5] Microwave assisted stereoselective synthesis of Cis-substituted TinIV phthalocyanine dicarboxylates.: Application as corrosion inhibitors [J].

Beltrán, HI ;

Esquivel, R ;

Sosa-Sánchez, A ;

Sosa-Sánchez, JL ;

Hopfl, H ;

Barba, V ;

Farfán, N ;

García, MG ;

Olivares-Xometl, O ;

Zamudio-Rivera, LS .

INORGANIC CHEMISTRY, 2004, 43 (12) :3555-3557

[6] Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 14-membered tetraaza macrocycles [J].

Biyiklioglu, Zekeriya ;

Kantekin, Halit ;

Oezil, Musa .

JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2007, 692 (12) :2436-2440

[7] Improvement in the synthesis of metallophthalocyanines using microwave irradiation [J].

Burczyk, A ;

Loupy, A ;

Bogdal, D ;

Petit, A .

TETRAHEDRON, 2005, 61 (01) :179-188

[8]

CAMMIDGE AN, 2005, CHEM COMMUN, V7930

[9] Synthesis, characterization, conduction and gas sensing properties of novel multinuclear metallo phthalocyanines (Zn, Co) with alkylthio substituents [J].

Ceyhan, T ;

Altindal, A ;

Erbil, MK ;

Bekaroglu, Ö .

POLYHEDRON, 2006, 25 (03) :737-746

[10] Phthalocyanines and phthalocyanine analogues:: The quest for applicable optical properties [J].

Claessens, CG ;

Blau, WJ ;

Cook, M ;

Hanack, M ;

Nolte, RJM ;

Torres, T ;

Wöhrle, D .

MONATSHEFTE FUR CHEMIE, 2001, 132 (01) :3-11

← 1 2 3 4 5 6 →