Characterization of fabricated cobalt-based alloy/nano bioactive glass composites

被引:6
作者
Bafandeh, Mohammad Reza [1 ]
Gharahkhani, Raziyeh [2 ]
Fathi, Mohammad Hossein [2 ]
机构
[1] Univ Kashan, Dept Mat Sci & Engn, Fac Engn, Kashan, Iran
[2] Isfahan Univ Technol, Dept Mat Engn, Esfahan 8415683111, Iran
来源
MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS | 2016年 / 69卷
关键词
Composite materials; Biomaterials; Sintering; Microstructure; Hydroxyapatite; IN-VITRO BIOACTIVITY; SOL-GEL; BONE-FORMATION; COATINGS; BIOGLASS; SURFACE; BIOMATERIALS; CERAMICS; BEHAVIOR; PROTEIN;
D O I
10.1016/j.msec.2016.07.053
中图分类号
TB3 [工程材料学]; R318.08 [生物材料学];
学科分类号
0805 ; 080501 ; 080502 ;
摘要
In this work, cobalt-based alloy/nano bioactive glass (NBG) composites with 10,15 and 20 wf% NBG were prepared and their bioactivity after immersion in simulated body fluid (SBF) for 1 to 4 weeks was studied. Scanning electron microscopy images of two-step sintered composites revealed relatively dense microstructure. The results showed that density of composite samples decreased with increase in NBG amount. The microstructure analysis as well as energy dispersive X-ray analysis (EDX) revealed that small amount of calcium phosphate phases precipitates on the surface of composite samples after 1 week immersion in SBF. After 2 weeks immersion, considerable amounts of cauliflower-like shaped precipitations were seen on the surface of the composites. Based on EDX analysis, these precipitations were composed mainly from Ca, P and Si. The observed bands in the Fourier transform infrared spectroscopy of immersed composites samples for 4 weeks in SBF, were characteristic bands of hydroxyapatite. Therefore it is possible to form hydroxyapatite layer on the surface of composite samples during immersion in SBF. The results indicated that prepared composites unlike cobalt-based alloy are bioactive, promising their possibility for implant applications. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:692 / 699
页数:8
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