Synthesis of pyrido[2,3-d:5,6-d']dipyrimidines using CuFe2O4/KCC-1/PMA as a novel and efficient nanocatalyst under solvent-free conditions

被引：14
作者：
Sadeghi, Seyyed Hojjat [1 ]
Yaghoobi, Morteza [2 ]
Ghasemzadeh, Mohammad Ali [2 ]
机构：
[1] Univ Kashan, Fac Basic Sci, Dept Chem, Kashan, Iran
[2] Islamic Azad Univ, Dept Chem, Qom Branch, Qom, Iran
来源：
APPLIED ORGANOMETALLIC CHEMISTRY | 2022年 / 36卷 / 08期
关键词：
CuFe2O4/KCC-1/PMA; heterogeneous catalyst; magnetic nanoparticles; multicomponent reactions; pyrido[2,3-d:5,6-d']dipyrimidines; POT MULTICOMPONENT SYNTHESIS; ACTIVATED ACETYLENES; DERIVATIVES; CATALYST; ANALOGS;
D O I：
10.1002/aoc.6771
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
In this research, the synthesis of pyrido[2,3-d:5,6-d']dipyrimidines by CuFe2O4/KCC-1/PMA magnetic nanoparticles was reported. Synthesis of pyrido[2,3-d:5,6-d']dipyrimidines was performed under solvent-free conditions with good to excellent yields. The prepared nanocatalyst was synthesized in three steps and also was characterized by Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), vibrating sample magnetometry (VSM), and N-2 adsorption-desorption measurement (Brunauer-Emmett-Teller [BET]) analyses. In addition, the reusability studies of CuFe2O4/KCC-1/PMA showed that the recovered catalyst could be used for several times.
引用
收藏
页数：10
相关论文
共 36 条
[1]  
Azizi N., 2021, RES CHEM INTERMEDIAT, V38, P2271
[2]   KCC-1 aminopropyl-functionalized supported on iron oxide magnetic nanoparticles as a novel magnetic nanocatalyst for the green and efficient synthesis of sulfonamide derivatives [J].
Azizi, Sajjad ;
Shadjou, Nasrin ;
Hasanzadeh, Mohammad .
APPLIED ORGANOMETALLIC CHEMISTRY, 2020, 34 (01)
[3]   Ecofriendly and Facile One-Pot Multicomponent Synthesis of 5-Phenyl-5,10-dihydropyrido[2,3-d: 6,5-d′]dipyrimidine-2,4,6,8(1H,3H,7H,9H)-tetraone Derivatives Catalyzed by CuII Immobilized on Functionalized Magnetic Mesoporous MCM-41 (Fe3O4@MCM-41-GPTMS-Gu-CuII) [J].
Baf, Mozhgan Mazloum Farsi ;
Akhlaghinia, Batool ;
Zarei, Zeinab ;
Ghodsinia, Sara S. E. .
CHEMISTRYSELECT, 2020, 5 (48) :15195-15208
[4]   Synthesis and characterization of a novel and green rod-like magnetic ZnS/CuFe2O4/agar organometallic hybrid catalyst for the synthesis of biologically-active 2-amino-tetrahydro-4H-chromene-3-carbonitrile derivatives [J].
Bahrami, Shahrzad ;
Hassanzadeh-Afruzi, Fereshte ;
Maleki, Ali .
APPLIED ORGANOMETALLIC CHEMISTRY, 2020, 34 (11)
[5]   PYRIDO[2,3-D]PYRIMIDINES .4. SYNTHETIC STUDIES LEADING TO VARIOUS OXOPYRIDO[2,3-D]PYRIMIDINES [J].
BROOM, AD ;
SHIM, JL ;
ANDERSON, GL .
JOURNAL OF ORGANIC CHEMISTRY, 1976, 41 (07) :1095-1099
[6]   Synthesis and biological evaluation of 3,6-diamino-1H-pyrazolo[3,4-b]pyridine derivatives as protein kinase inhibitors [J].
Chioua, Mourad ;
Samadi, Abdelouahid ;
Soriano, Elena ;
Lozach, Olivier ;
Meijer, Laurent ;
Marco-Contelles, Jose .
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2009, 19 (16) :4566-4569
[7]   Ruthenium (III) chloride as a novel and efficient catalyst for the synthesis of substituted pyrroles under solvent-free conditions [J].
De, Surya K. .
CATALYSIS LETTERS, 2008, 124 (3-4) :174-177
[8]   N-propylbenzoguanamine sulfonic acid-functionalized magnetic nanoparticles: A novel and magnetically retrievable catalyst for the synthesis of 1,4-dihydropyridine derivatives [J].
Dehbalaei, Masoumeh Gholami ;
Foroughifar, Naser ;
Khajeh-Amiri, Alireza ;
Pasdar, Hoda .
JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2018, 65 (11) :1356-1369
[9]  
Deyanov A., 1991, PHARM CHEM J, V25, P248
[10]   SYNTHESIS AND ANTIMICROBIAL ACTIVITY OF 6,7-ANNULATED PYRIDO[2,3-D]PYRIMIDINES [J].
DONKOR, IO ;
KLEIN, CL ;
LIANG, L ;
ZHU, NJ ;
BRADLEY, E ;
CLARK, AM .
JOURNAL OF PHARMACEUTICAL SCIENCES, 1995, 84 (05) :661-664
1234