Acylation of aliphatic diamines with methyl nitroacetate

被引：1
|
作者：
Lyapkalo, IM [1 ]
Ioffe, SL [1 ]
Strelenko, YA [1 ]
Tartakovsky, VA [1 ]
机构：
[1] ND ZELINSKII INST ORGAN CHEM,MOSCOW 117913,RUSSIA
来源：
RUSSIAN CHEMICAL BULLETIN | 1996年 / 45卷 / 09期
关键词：
methyl nitroacetate; N; N'-bis(nitroacetyl)diamines; aminolysis; nucleophilic catalysis;
D O I：
10.1007/BF01430754
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
N,N'-Bis(nitroacetyl)diamines were synthesized for the first time by the reaction of methyl nitroacetate with aliphatic diamines in H2O or EtOH in the presence of pyridine or imidazole. In the case of 1,2-ethylenediamine, the N-mononitroacetyl derivative was isolated as an intermediate product.
引用
收藏
页码：2245 / 2247
页数：3
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