The measurement of the tip current noise as a method to characterize the exposed area of coated ESTM tips

被引:7
作者
Abadal, G [1 ]
Pérez-Murano, F [1 ]
Barniol, N [1 ]
Aymerich, X [1 ]
机构
[1] Univ Autonoma Barcelona, Dept Elect Engn, E-08193 Barcelona, Spain
关键词
current noise; electrochemical scanning tunneling microscopy; (ESTM) tip coating; exposed tip area; nanotechnology; scanning probe microscopy; ultramicroelectrodes;
D O I
10.1109/TIM.2003.814683
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
A new method to characterize the uncoated area of electrochemical scanning tunneling microscopy (ESTM) tips based on the measurement of the rms tip current noise is presented. A clear relationship between this noise and the exposed area measured by means of different standard techniques is shown. A simple model based on the tip-electrolyte system allows adjustment of the relationship. The new technique is,advantageous with respect to the standard methods because it is nondestructive and because it can be applied in situ during an ESTM experiment, allowing continuous monitoring of the tip coating state.
引用
收藏
页码:859 / 864
页数:6
相关论文
共 13 条
[1]   Field induced oxidation of silicon by SPM: study of the mechanism at negative sample voltage by STM, ESTM and AFM [J].
Abadal, G ;
Perez-Murano, F ;
Barniol, N ;
Aymerich, X .
APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 1998, 66 (Suppl 1) :S791-S795
[2]   Electrochemical modifications at the nanometer scale on Si(100) surfaces with scanning tunnelling microscopy [J].
Abadal, G ;
Perez-Murano, F ;
Barniol, N ;
Aymerich, X .
THIN SOLID FILMS, 1998, 317 (1-2) :493-496
[3]  
ABADAL G, THESIS U AUTONOMA BA
[4]  
[Anonymous], 1990, Introduction to communication systems
[5]  
BARD AJ, 1980, ELECTROCHEMICAL METH
[6]   SURFACE STUDIES BY SCANNING TUNNELING MICROSCOPY [J].
BINNING, G ;
ROHRER, H ;
GERBER, C ;
WEIBEL, E .
PHYSICAL REVIEW LETTERS, 1982, 49 (01) :57-61
[7]   FABRICATION AND CHARACTERIZATION OF MICROTIPS FOR INSITU SCANNING TUNNELING MICROSCOPY [J].
GEWIRTH, AA ;
CRASTON, DH ;
BARD, AJ .
JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 1989, 261 (2B) :477-482
[8]   PREPARATION OF STM TIPS FOR INSITU CHARACTERIZATION OF ELECTRODE SURFACES [J].
HEBEN, MJ ;
DOVEK, MM ;
LEWIS, NS ;
PENNER, RM ;
QUATE, CF .
JOURNAL OF MICROSCOPY, 1988, 152 :651-661
[9]  
MOLLER R, 1989, APPL PHYS LETT, V55, P2360, DOI 10.1063/1.102018
[10]   PREPARATION AND CHARACTERIZATION OF STM TIPS FOR ELECTROCHEMICAL STUDIES [J].
NAGAHARA, LA ;
THUNDAT, T ;
LINDSAY, SM .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1989, 60 (10) :3128-3130