Finding the energy source for self-propagating high-temperature synthesis production of NiTi shape memory alloy

被引:13
作者
Novak, Pavel [1 ]
Skolakova, Andrea [1 ]
Pignol, Damien [1 ]
Prusa, Filip [1 ]
Salvetr, Pavel [1 ]
Kubatik, Tomas Frantisek [2 ]
Perriere, Loic [3 ,4 ]
Karlik, Miroslav [5 ]
机构
[1] Univ Chem & Technol, Dept Met & Corros Engn, Tech 5, Prague 16628 6, Czech Republic
[2] Inst Plasma Phys AS CR, Vvi, Slovankou 3, Prague 18200 8, Czech Republic
[3] CNRS, UMR 7182, ICMPE, 2-8 Rue Henri Dunant, F-94320 Thiais, France
[4] Univ Paris Est Creteil, 2-8 Rue Henri Dunant, F-94320 Thiais, France
[5] Czech Tech Univ, Fac Nucl Sci & Phys Engn, Dept Mat, Trojanova 13, Prague 12000 2, Czech Republic
关键词
NiTi; Shape memory alloys; Powder metallurgy; Microstructure; COMBUSTION SYNTHESIS; SHS; MICROSTRUCTURE;
D O I
10.1016/j.matchemphys.2016.06.062
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Our previous works on the synthesis of intermetallics by Self-propagating High-temperature Synthesis revealed strong dependence of microstructure of the products on heating rate. In this paper, the application of various heating regimes and sources was tested in preparation of Ni-Ti shape memory alloy. It was found that high heating rate (approx. over 100 degrees C min(-1)) was required to obtain the material with maximized amount of NiTi shape memory phase and no unreacted metals. Heating in electric resistance furnace preheated to the process temperature or induction heating furnace seemed to be promising for this purpose. On the other hand, Spark Plasma Sintering was found to be inapplicable, because the strongest increase of the temperature occurred on the surface of the particles, producing layers of intermetallics that further acted as diffusion barriers. (C) 2016 Elsevier B.V. All rights reserved.
引用
收藏
页码:295 / 300
页数:6
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