Electrocatalytic oxidation of hydrazine at a glassy carbon electrode modified with nickel ferrite and multi-walled carbon nanotubes

被引:26
|
作者
Fang, Bin [1 ]
Feng, Yuehua [1 ]
Liu, Min [1 ]
Wang, Guangfeng [1 ]
Zhang, Xiaojun [2 ]
Wang, Meifang [3 ]
机构
[1] Anhui Normal Univ, Coll Chem & Mat Sci, Anhui Key Lab Chemobiosensing, Wuhu 241000, Peoples R China
[2] Anhui Normal Univ, Coll Chem & Mat Sci, Anhui Key Lab Funct Mol Solids, Wuhu 241000, Peoples R China
[3] Wannan Med Coll, Dept Chem, Wuhu 241000, Peoples R China
基金
中国国家自然科学基金;
关键词
Nickel ferrite; MWCNTs; Modified electrode; Electrocatalysis; Hydrazine; SEMICONDUCTING GAS SENSOR; AMPEROMETRIC DETECTION; CERAMIC ELECTRODE; MICRODISK ARRAY; NANOPARTICLES; NANOCRYSTALS; ENHANCEMENT; VOLTAMMETRY; COMPOSITES; DEPOSITION;
D O I
10.1007/s00604-011-0662-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A hydrothermal technique was used to synthesize nickel ferrite nanoparticles (NF-NPs) deposited on multi-walled carbon nanotubes (MWCNTs). The material was characterized by scanning electron microscopy, energy dispersive spectrometry, and X-ray powder diffraction which showed that the NF-NPs are located on the surface of the carboxylated MWCNTs. The material was used to modify a glassy carbon electrode which then was characterized via cyclic voltammetry, electrochemical impedance spectroscopy, and amperometry. The electrode displays strong electrochemical response to hydrazine. A potential hydrazine sensing scheme is suggested.
引用
收藏
页码:145 / 150
页数:6
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