Preparation and characterization of polyimide/silica nanocomposite spheres

被引:27
作者
Liu, Qiu-Ping [1 ]
Gao, Ling-Xiang [1 ]
Gao, Zi-Wei [1 ]
Yang, Lin [1 ]
机构
[1] Shaanxi Normal Univ, Sch Chem & Mat Sci, Key Lab Macromol Sci Shaanxi Province, Xian 710062, Peoples R China
关键词
polyimide; silica; nanocomposites; coated particles; composite materials;
D O I
10.1016/j.matlet.2007.02.022
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Silica (SiO2) nanocomposite spherical particles coated with polyimide had been synthesized by a dispersion polymerization method. The chemical structure of polyimide/silica (PI/SiO2) nanocomposite spherical particles was investigated by using FT-IR, and the surface morphology characterization was performed with SEM. The TEM showed that SiO2 core was surface-coated with a multilayer composite and the multilayer thickness was about 20 nm. Moreover, the particles were homogeneously distributed and interconnected very fine. Basing the results, it was found that the PI/SiO2 nanocomposite particles were core-shell structure. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:4456 / 4458
页数:3
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