Using Taguchi Robust Design Method to Develop an Optimized Synthesis Procedure for Nanocrystals of ZSM-5 Zeolite

被引：19
|
作者：
Abrishamkar, Maryam [1 ]
Azizi, Seyed Naser [1 ]
Kazemian, Hossein [2 ]
机构：
[1] Univ Mazandaran, Analyt Div, Fac Chem, Babol Sar, Iran
[2] Univ Western Ontario, Dept Chem & Biochem Engn, Fac Engn, London, ON N6A 5B9, Canada
来源：
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE | 2011年 / 637卷 / 01期
关键词：
Taguchi method; Nanoparticles; Zeolites; Synthesis design; X-ray diffraction; NUCLEATION PERIOD; CRYSTALLIZATION; TPA-SILICALITE-1; CRYSTALLINITY; SILICALITE-1; FILMS;
D O I：
10.1002/zaac.201000202
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The effects of TPAOH/SiO2, H2O/SiO2, SiO2/Na2O and SiO2/Al2O3 ratios in the initial synthetic mixture on the crystallization of nanoparticles of ZSM-5 zeolite under atmospheric pressure were studied. A Taguchi orthogonal experimental design with three levels of the above-mentioned parameters was used to optimize the experiment parameters by the analysis of variances (ANOVA). Applying the Taguchi method significantly reduced the time and cost for optimization. The obtained products were characterized by scanning electron microscopy, X-ray diffraction and FT-IR spectroscopy. As a result of the Taguchi analysis TPAOH/SiO2 followed by SiO2/Al2O3 was the most influencing parameters for the synthesis of nanosized ZSM-5 crystals.
引用
收藏
页码：154 / 159
页数：6
相关论文
共 50 条
  • [1] Applying the Taguchi Method to Develop an Optimized Synthesis Procedure for Nanocrystals of T-Type Zeolite
    Matin, Kianoosh Tehrani
    Bastani, Dariush
    Kazemian, Hossein
    CHEMICAL ENGINEERING & TECHNOLOGY, 2009, 32 (07) : 1042 - 1048
  • [2] Using Taguchi robust design method to develop an optimized synthesis procedure of nanocrystalline cancrinite
    Azizi, Seyed Naser
    Asemi, Neda
    Samadi-Maybodi, Abdolraouf
    INTERNATIONAL CONFERENCE ON FUNDAMENTAL AND APPLIED SCIENCES 2012 (ICFAS2012), 2012, 1482 : 568 - 571
  • [3] Synthesis of Micro/Mesoporous Zeolite ZSM-5 Using a Natural Aluminosilicate
    R. Z. Kuvatova
    O. S. Travkina
    B. I. Kutepov
    Catalysis in Industry, 2021, 13 : 99 - 104
  • [4] Synthesis of Micro/Mesoporous Zeolite ZSM-5 Using a Natural Aluminosilicate
    Kuvatova, R. Z.
    Travkina, O. S.
    Kutepov, B. I.
    CATALYSIS IN INDUSTRY, 2021, 13 (02) : 99 - 104
  • [5] Synthesis of nanosized ZSM-5 zeolite with intracrystalline mesopores
    Xue, Zhaoteng
    Ma, Jinghong
    Zhang, Tuo
    Miao, Haixia
    Li, Ruifeng
    MATERIALS LETTERS, 2012, 68 : 1 - 3
  • [6] Synthesis of zeolite ZSM-5: Effect of emulsifiers
    Chauhan, Nilam L.
    Das, Jagannath
    Jasra, Raksh V.
    Murthy, Z. V. P.
    Parikh, Parimal A.
    CRYSTAL RESEARCH AND TECHNOLOGY, 2012, 47 (07) : 746 - 753
  • [7] The synthesis of nano-sized ZSM-5 zeolite by dry gel conversion method and investigating the effects of experimental parameters by Taguchi experimental design
    Mohammadparast, Farshid
    Halladj, Rouein
    Askari, Sima
    JOURNAL OF EXPERIMENTAL NANOSCIENCE, 2018, 13 (01) : 160 - 173
  • [8] Template-Free Synthesis of Hierarchical Zeolite ZSM-5
    Shestakova, D. O.
    Sashkina, K. A.
    Parkhomchuk, E., V
    PETROLEUM CHEMISTRY, 2019, 59 (08) : 838 - 844
  • [9] Continuous flow synthesis of ZSM-5 zeolite on the order of seconds
    Liu, Zhendong
    Okabe, Kotatsu
    Anand, Chokkalingam
    Yonezawa, Yasuo
    Zhu, Jie
    Yamada, Hiroki
    Endo, Akira
    Yanaba, Yutaka
    Yoshikawa, Takeshi
    Ohara, Koji
    Okubo, Tatsuya
    Wakihara, Toru
    PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2016, 113 (50) : 14267 - 14271
  • [10] Calculation of the properties of acid sites of the zeolite ZSM-5 using ONIOM method
    Sillar, K
    Burk, P
    JOURNAL OF MOLECULAR STRUCTURE-THEOCHEM, 2002, 589 : 281 - 290
12345