{2-[(Benzoyloxy)methyl]-1-oxo-3H-pyrrolizin-2-yl}methyl benzoate

被引：0
|
作者：
Ali, Yousaf [1 ]
Yousuf, Sammer [2 ]
Afza, Nighat [1 ]
Peng, Yu [3 ]
Kalhoro, Mahboob Ali [1 ]
机构：
[1] PCSIR Labs Complex, Pharmaceut Res Ctr, Karachi 75280, Pakistan
[2] Univ Karachi, HEJ Res Inst Chem, Int Ctr Chem & Biol Sci, Karachi 75270, Pakistan
[3] Tianjin Univ Sci & Technol, Dept Pharmaceut Engn, Biotechnol Coll, Tianjin 300457, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
D O I：
10.1107/S1600536810051974
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C23H19NO5, was prepared by esterification of 2,2-bis(hydroxymethyl)-2,3-dihydro-1H-pyrrolizin-1-one with benzoyl chloride in pyridine. The pyrrolizine ring system is approximately planar with a maximum deviation of 0.008 (2) angstrom from the least-squares plane; the two phenyl rings are oriented at dihedral angles of 64.26 (11) and 70.75 (10)degrees with respect to the pyrrolizine ring system. Weak intermolecular C-H center dot center dot center dot O hydrogen bonding occurs in the crystal structure.
引用
收藏
页码：O172 / U2878
页数：14
相关论文
共 50 条
  • [21] Dimethyl 2-(1-Methyl-3-oxo-1,3-dihydroisobenzofuran-1-yl)malonate
    Di Mola, Antonia
    Filosa, Rosanna
    Massa, Antonio
    MOLBANK, 2020, 2020 (02)
  • [22] Methyl 2-(5-methyl-3-methylsulfinyl-1-benzofuran-2-yl)acetate
    Choi, Hong Dae
    Seo, Pil Ja
    Son, Byeng Wha
    Lee, Uk
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1711 - U1528
  • [23] Aqueous hydrolysis of 3-[2-(3-methyl-1H-pyrazol-1-yl)-ethylamino]-and 3-[2-(5-methyl-1H-pyrazol-1-yl)ethylamino]-propanoates
    O. S. Attaryan
    A. O. Balayan
    G. B. Asratyan
    Russian Journal of General Chemistry, 2008, 78 : 1425 - 1426
  • [24] Aqueous hydrolysis of 3-[2-(3-methyl-1H-pyrazol-1-yl)-ethylamino]- and 3-[2-(5-methyl-1H-pyrazol-1-yl)ethylamino]-propanoates
    Attaryan, O. S.
    Balayan, A. O.
    Asratyan, G. B.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2008, 78 (07) : 1425 - 1426
  • [25] Ethyl 2-(benzoyloxy)benzoate
    Iqbal, Rashid
    Zareef, Muhammad
    Aziz, Saeeda
    Qadeer, Ghulam
    Arfan, Muhammad
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O744 - O745
  • [26] Synthesis,Crystal Structure and Neuroprotection of Methyl 2-((4-(2-(2-Methylphenoxy)acetyl)-piperazin-1-yl)-methyl)benzoate
    仲琰
    王垚
    王晶
    许逸
    李萍
    吴斌
    结构化学, 2014, 33 (07) : 1096 - 1101
  • [27] Methyl {2-[4-ethyl-1-(tolylsulfonyl)-2,3-dihydropyrrol-3-yl]ethyl}benzoate
    Hu, YM
    Li, YZ
    Zhou, J
    Hu, HW
    Pan, Y
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1578 - O1580
  • [28] 2-{[2-(Pyridin-4-yl)-1H-benzimidazol-1-yl] methyl} phenol
    Omer, Mohammed A. S.
    Liu, Jia-Cheng
    Xiao, Chao-Hu
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O700 - +
  • [29] 2-[(1H-Pyrrol-2-yl)methyl]-1H-pyrrole
    Kim, Chong-Hyeak
    Jeon, Yea-Sel
    Lynch, Vincent
    Sessler, Jonathan L.
    Hwang, Kwang-Jin
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1697 - +
  • [30] Synthesis, characterization and crystal structure of methyl 2-(2-oxo-2H-chromen-4-ylamino)benzoate
    Hollauer, Henrique V. P.
    Vilas Novas, Rachel C.
    Guedes, Guilherme P.
    Buarque, Camilla D.
    Escobar, Livia B. L.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2023, 79 : 842 - +
12345