GISAXS Analysis for Ionomer Thin Films

被引：1
作者：
Dudenas, P. [1 ,2 ]
Kusoglu, A. [2 ]
Hexemer, A. [2 ]
Weber, A. [2 ]
机构：
[1] Univ Calif Berkeley, Dept Chem Engn, Berkeley, CA 94720 USA
[2] Lawrence Berkeley Natl Lab, 1 Cyclotron Rd, Berkeley, CA 94720 USA
来源：
POLYMER ELECTROLYTE FUEL CELLS 16 (PEFC 16) | 2016年 / 75卷 / 14期
关键词：
X-RAY-SCATTERING; POLYMER-FILMS; NAFION FILMS; ANGLE; MEMBRANES;
D O I：
10.1149/07514.0643ecst
中图分类号：
O646 [电化学、电解、磁化学];
学科分类号：
081704 ;
摘要：
An overview of GISAXS analysis for ionomer thin films is presented. Experimental procedures to prepare and measure thin films using GISAXS is described. Typical features of ionomer scattering images are discussed before detailing three different types of analysis which can be used in conjunction with one another to elucidate additional information from scattering patterns. Example data are provided to illustrate these techniques.
引用
收藏
页码：643 / 650
页数：8
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  • [1] Morphology of Hydrated As-Cast Nafion Revealed through Cryo Electron Tomography
    Allen, Frances I.
    Comolli, Luis R.
    Kusoglu, Ahmet
    Modestino, Miguel A.
    Minor, Andrew M.
    Weber, Adam Z.
    [J]. ACS MACRO LETTERS, 2015, 4 (01): : 1 - 5
  • [2] Electrospinning and solution properties of Nafion and poly(acrylic acid)
    Chen, Hong
    Snyder, Joshua D.
    Elabd, Yossef A.
    [J]. MACROMOLECULES, 2008, 41 (01) : 128 - 135
  • [3] Interpretation of the small-angle X-ray scattering from swollen and oriented perfluorinated ionomer membranes
    Elliott, JA
    Hanna, S
    Elliott, AMS
    Cooley, GE
    [J]. MACROMOLECULES, 2000, 33 (11) : 4161 - 4171
  • [4] SMALL-ANGLE X-RAY-SCATTERING STUDY OF PERFLUORINATED IONOMER MEMBRANES .1. ORIGIN OF 2 SCATTERING MAXIMA
    FUJIMURA, M
    HASHIMOTO, T
    KAWAI, H
    [J]. MACROMOLECULES, 1981, 14 (05) : 1309 - 1315
  • [5] THE MORPHOLOGY IN NAFION PERFLUORINATED MEMBRANE PRODUCTS, AS DETERMINED BY WIDE-ANGLE AND SMALL-ANGLE X-RAY STUDIES
    GIERKE, TD
    MUNN, GE
    WILSON, FC
    [J]. JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 1981, 19 (11) : 1687 - 1704
  • [6] Subsecond Morphological Changes in Nafion during Water Uptake Detected by Small-Angle X-ray Scattering
    Kusoglu, Ahmet
    Modestino, Miguel A.
    Hexemer, Alexander
    Segalman, Rachel A.
    Weber, Adam Z.
    [J]. ACS MACRO LETTERS, 2012, 1 (01) : 33 - 36
  • [7] Structural characterization using the multiple scattering effects in grazing-incidence small-angle X-ray scattering
    Lee, Byeongdu
    Lo, Chieh-Tsung
    Thiyagarajan, P.
    Lee, Dong R.
    Niu, Zhongwei
    Wang, Qian
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2008, 41 : 134 - 142
  • [8] State of understanding of Nafion
    Mauritz, KA
    Moore, RB
    [J]. CHEMICAL REVIEWS, 2004, 104 (10) : 4535 - 4585
  • [9] Self-Assembly and Transport Limitations in Confined Nafion Films
    Modestino, Miguel A.
    Paul, Devproshad K.
    Dishari, Shudipto
    Petrina, Stephanie A.
    Allen, Frances I.
    Hickner, Michael A.
    Karan, Kunal
    Segalman, Rachel A.
    Weber, Adam Z.
    [J]. MACROMOLECULES, 2013, 46 (03) : 867 - 873
  • [10] Correlated roughness, long-range correlations, and dewetting of thin polymer films
    Muller-Buschbaum, P
    Stamm, M
    [J]. MACROMOLECULES, 1998, 31 (11) : 3686 - 3692
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