A one-pot, solid-phase synthesis of secondary amines from reactive alkyl halides and an alkyl azide

被引:19
|
作者
Ayesa, Susana [1 ]
Samuelsson, Bertil [1 ]
Classon, Bjorn [1 ]
机构
[1] Medivir AB, S-14122 Huddinge, Sweden
关键词
secondary amines; azides; phosphinimine; polymer-supported triphenylphosphine; alkylation;
D O I
10.1055/s-2007-990927
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A one-pot, two-step, polymer-bound, triphenylphosphine-supported synthesis of secondary amines from the corresponding azide and a reactive alkyl halide is described.
引用
收藏
页码:97 / 99
页数:3
相关论文
共 50 条
  • [1] One-pot preparation of alkyl halides from alkyl diphenylphosphinites
    Ruchamanee, Kanokporn
    Chavasiri, Warinthon
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2010, 240
  • [2] A ONE-POT SYNTHESIS OF KETENE DITHIOACETALS FROM ALKYL-HALIDES
    KAYA, R
    BELLER, NR
    SYNTHESIS-STUTTGART, 1981, (10): : 814 - 816
  • [3] One-pot synthesis of functionalized thioureas by reaction of benzoyl isothiocyanates, secondary amines, and alkyl propiolates
    Yavari, Issa
    Sayyed-Alangi, S. Zahra
    Sabbaghan, Maryam
    Hajinasiri, Rahimeh
    Iravani, Nasir
    MONATSHEFTE FUR CHEMIE, 2008, 139 (09): : 1025 - 1028
  • [4] One-pot synthesis of functionalized thioureas by reaction of benzoyl isothiocyanates, secondary amines, and alkyl propiolates
    Issa Yavari
    S. Zahra Sayyed-Alangi
    Maryam Sabbaghan
    Rahimeh Hajinasiri
    Nasir Iravani
    Monatshefte für Chemie - Chemical Monthly, 2008, 139 : 1025 - 1028
  • [5] Sequential One-Pot Ruthenium-Catalyzed Azide-Alkyne Cycloaddition from Primary Alkyl Halides and Sodium Azide
    Johansson, Johan R.
    Lincoln, Per
    Norden, Bengt
    Kann, Nina
    JOURNAL OF ORGANIC CHEMISTRY, 2011, 76 (07): : 2355 - 2359
  • [6] One-pot and simple reaction for the synthesis of alkyl p-toluenesulfinate esters under solid-phase conditions
    Hajipour, AR
    Mallakpour, SE
    Afrousheh, A
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2000, 160 : 67 - 75
  • [7] ONE-POT SYNTHESIS OF ALKYL ARYL TRITHIOCARBONATES FROM BENZENETHIOLS, ALKYL-HALIDES, AND CARBON-DISULFIDE WITH A PHASE-TRANSFER CATALYST
    SUGAWARA, A
    SHIRAHATA, M
    SATO, S
    SATO, R
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1984, 57 (11) : 3353 - 3354
  • [8] An efficient, basic resin mediated, one-pot synthesis of dithiocarbazates from the corresponding alkyl halides
    Chaturvedi, Devdutt
    Mishra, Nisha
    Mishra, Virendra
    JOURNAL OF SULFUR CHEMISTRY, 2008, 29 (05) : 503 - 509
  • [9] One-Pot Synthesis of 5-Alkylsulfanyl-1H-tetrazoles from Alkyl Halides
    Myznikov, L. V.
    Vorona, S. V.
    Artamonova, T. V.
    Zevatskii, Yu. E.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2017, 87 (06) : 1313 - 1316
  • [10] A FACILE ONE-POT SYNTHESIS OF SULFIDES FROM ALKYL-HALIDES AND ALCOHOLS USING TETRAMETHYLTHIOUREA
    FUJISAKI, S
    FUJIWARA, I
    NORISUE, Y
    KAJIGAESHI, S
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1985, 58 (08) : 2429 - 2430