Growth and properties of organic nonlinear optical crystals: L-tartaric acid-nicotinamide and D-tartaric acid-nicotinamide

被引：24

作者：

Shen, J ^{[1
]}

Zheng, JM ^{[1
]}

Che, YX ^{[1
]}

Xi, B ^{[1
]}

机构：

[1] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2003年 / 257卷 / 1-2期

关键词：

solubility curves; solvent; single crystal growth; solution growth; organic compounds; nonlinear optics;

D O I：

10.1016/S0022-0248(03)01408-8

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Two novel single crystals Of L-tartaric acid-nicotinamide (LTN, 2HOOC HC(OH)HC(OH)COO-.2C(5)H(4)NH(+) CONH2.H2O,) and D-tartaric acid Nicotinamide (DTN, 2HOOCHC(OH)HC(OH)COO-.2C(5)H(4)NH(+)CONH(2).H2O), good quality organic nonlinear optical (NLO) materials have been successfully grown by the temperature lowering method from aqueous solution. Solubility curves of both LTN and DTN have been determined in water. The solubility of both LTN and DTN steadily moved upward along with the uninterrupted rise of the solution temperature. Effects of different solvents on growth of LTN and DTN single crystals were compared. The LTN single crystal in size 12 x 42 x 2 mm(3) was grown in the deionized water for 5 days while DTN single crystal in size 28 x 12 x 3 mm(3) was grown for only 12 h. The transmission ranges of both LTN and DTN single crystals have been found to be between 280 and 1900nm. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：136 / 140

页数：5

共 8 条

[1] Solution growth of a novel nonlinear optical material: L-histidine tetrafluoroborate [J].

Aggarwal, MD ;

Choi, J ;

Wang, WS ;

Bhat, K ;

Lal, RB ;

Shields, AD ;

Penn, BG ;

Frazier, DO .

JOURNAL OF CRYSTAL GROWTH, 1999, 204 (1-2) :179-182

[2] 2ND-HARMONIC GENERATION IN AROMATIC ORGANIC-COMPOUNDS [J].

FRAZIER, CC ;

COCKERHAM, MP ;

CHAUCHARD, EA ;

LEE, CH .

JOURNAL OF THE OPTICAL SOCIETY OF AMERICA B-OPTICAL PHYSICS, 1987, 4 (11) :1899-1903

[3] L-HISTIDINE TETRAFLUOROBORATE - A SOLUTION-GROWN SEMIORGANIC CRYSTAL FOR NONLINEAR FREQUENCY-CONVERSION [J].

MARCY, HO ;

ROSKER, MT ;

WARREN, LF ;

CUNNINGHAM, PH ;

THOMAS, CA ;

DELOACH, LA ;

VELSKO, SP ;

EBBERS, CA ;

LIAO, JH ;

KANATZIDIS, MG .

OPTICS LETTERS, 1995, 20 (03) :252-254

[4]

Reichardt C., 2010, Solvents and Solvent Effect in Organic Chemistry

[5] SELECTION OF SOLVENTS FOR ORGANIC-CRYSTAL GROWTH FROM SOLUTION [J].

TANAKA, Y ;

MATSUOKA, M .

JOURNAL OF CRYSTAL GROWTH, 1990, 99 (1-4) :1130-1133

[6]

VINSHTEIN BK, 1981, MODERN CRYSTALLOGRAP, V1, P155

[7] Rapid growth of hybrid organic-inorganic crystals for nonlinear optics [J].

Zaccaro, J ;

Härtwig, J ;

Baruchel, J ;

Ibanez, A .

JOURNAL OF CRYSTAL GROWTH, 1999, 204 (03) :325-332

[8] GROWTH OF LARGE METHYL-(2,4-DINITROPHENYL)-AMINOPROPANOATE - 2-METHYL-4-NITROANILINE CRYSTALS FOR NONLINEAR-OPTICAL APPLICATIONS [J].

ZHANG, HW ;

BATRA, AK ;

LAL, RB .

JOURNAL OF CRYSTAL GROWTH, 1994, 137 (1-2) :141-144

← 1 →