Preparation of artificially spiked soil with polycyclic aromatic hydrocarbons for soil pollution analysis

被引：18

作者：

Sawada, A ^{[1
]}

Kanai, K ^{[1
]}

Fukushima, M ^{[1
]}

机构：

[1] Natl Inst Adv Ind Sci & Technol, Tsukuba, Ibaraki 3058569, Japan

来源：

ANALYTICAL SCIENCES | 2004年 / 20卷 / 01期

关键词：

D O I：

10.2116/analsci.20.239

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

To confirm the method for preparing artificially spiked soil with polycyclic aromatic hydrocarbons (PAHs), we tested the homogeneity of PAHs in spiked soils, which were prepared by three different procedures, by using kaolin and ando soil. When the slurry of kaolin and acetone containing PAHs were evaporated by a rotary evaporator at 30 - 35degreesC, the most homogeneous distribution of PAHs was obtained in the spiked soil. This procedure was applied to the preparation of PAH-spiked soil for natural soil (ando soil). Such spiked soils can be useful as the standard materials for standardization of the analytical methods for PAHs in the soil and sediment samples.

引用

页码：239 / 241

页数：3

共 14 条

[1]

AYRIS S, 1997, ORGANOHALOGEN COMPOU, V33, P250

[2] Comparison of different drying, extraction and detection techniques for the determination of priority polycyclic aromatic hydrocarbons in background contaminated soil samples [J].

Berset, JD ;

Ejem, M ;

Holzer, R ;

Lischer, P .

ANALYTICA CHIMICA ACTA, 1999, 383 (03) :263-275

[3] Characterization and FATE of PAH-contaminated sediments at the Wyckoff/Eagle Harbor superfund site [J].

Brenner, RC ;

Magar, VS ;

Ickes, JA ;

Abbott, JE ;

Stout, SA ;

Crecelius, EA ;

Bingler, LS .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2002, 36 (12) :2605-2613

[4] Contaminant risks from biosolids land application: Contemporary organic contaminant levels in digested sewage sludge from five treatment plants in Greater Vancouver, British Columbia [J].

Bright, DA ;

Healey, N .

ENVIRONMENTAL POLLUTION, 2003, 126 (01) :39-49

[5]

FUKUSHIMA M, IN PRESS TOXICOL ENV

[6] Sorption of pyrene to dissolved humic substances and related model polymers. 1. Structure-property correlation [J].

Kopinke, FD ;

Georgi, A ;

MacKenzie, K .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2001, 35 (12) :2536-2542

[7] MEASURED AND ESTIMATED VOLATILIZATION OF NAPHTHALENE FROM A SANDY SOIL [J].

LINDHARDT, B ;

CHRISTENSEN, TH .

CHEMOSPHERE, 1994, 29 (07) :1407-1419

[8] Partitioning, extractability, and formation of nonextractable PAH residues in soil. 1. Compound differences in aging and sequestration [J].

Northcott, GL ;

Jones, KC .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2001, 35 (06) :1103-1110

[9] Solid-solution partitioning of organic matter in soils as influenced by an increase in pH or Ca concentration [J].

Oste, LA ;

Temminghoff, EJM ;

Van Riemsdijk, WH .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 2002, 36 (02) :208-214

[10] Relationships between structure and binding affinity of humic substances for polycyclic aromatic hydrocarbons: Relevance of molecular descriptors [J].

Perminova, IV ;

Grechishcheva, NY ;

Petrosyan, VS .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1999, 33 (21) :3781-3787

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