Preparation and characterization of nanocrystalline PbSe in poly(acrylic acid-co-styrene)

被引：8
|
作者：
Sun, YY [1 ]
Qian, XF [1 ]
Yin, J [1 ]
Huang, JC [1 ]
Ma, XD [1 ]
Zhu, ZK [1 ]
机构：
[1] Shanghai Jiao Tong Univ, Sch Chem & Chem Technol, Res Inst Polymer Mat, Shanghai 200240, Peoples R China
来源：
JOURNAL OF MATERIALS RESEARCH | 2001年 / 16卷 / 10期
关键词：
D O I：
10.1557/JMR.2001.0401
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The in situ reduction method was used to prepare nanocrystalline PbSe in a poly(acrylic acid-co-styrene) matrix. Metal precursor-doped polymer film was treated with selenium and reducing reagent (NaBH4) in ethylenediamine, leading to the formation of assemblies of crystalline semiconductive PbSe in polymer. The preparation was done at room temperature and ambient pressure. X-ray diffraction, x-ray photoelectron spectroscopy, infrared, scanning electron microscopy, transmission electron microscopy, and ultraviolet-visible spectra were used to characterize the as-prepared materials. The key factor for successful preparation of this composite was also discussed.
引用
收藏
页码：2922 / 2927
页数：6
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