p-Nitrobenzaldehyde nicotinoylhydrazone monohydrate

被引：28

作者：

Lu, ZL ^{[1
]}

Duan, CY ^{[1
]}

Tian, YP ^{[1
]}

You, XZ ^{[1
]}

Fun, HK ^{[1
]}

Sivakumar, K ^{[1
]}

机构：

[1] UNIV SAINS MALAYSIA,SCH PHYS,XRAY CRYSTALLOG UNIT,GEORGE TOWN,MALAYSIA

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1996年 / 52卷

关键词：

D O I：

10.1107/S0108270195016702

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The X-ray analysis revealed that the title compound, C13H10N4O3.H2O, is a practically planar molecule which exists in the keto tautomeric form. The molecules lie parallel to (022) planes and form centrosymmetrically related dimers with possible pi interactions. The water molecule bridges the hydrazone molecules of the adjacent stacks through hydrogen bonds and the crystal structure is stabilized by O-H ... O, N-H ... O and C-H ... O hydrogen bonds.

引用

页码：1507 / 1509

页数：3

共 10 条

[1] THE PREPARATION AND COORDINATION CHEMISTRY OF 2,6-DIACETYLPYRIDINE BIS(6-CHLORO-2-PYRIDYLHYDRAZONE) [J].

CONSTABLE, EC ;

HOLMES, JM .

INORGANICA CHIMICA ACTA, 1987, 126 (02) :187-193

[2]

DUTTA RL, 1985, J SCI IND RES INDIA, V44, P635

[3] p-(Dimethylamino)benzaldehyde isonicotinoylhydrazone monohydrate [J].

Fun, HK ;

Sivakumar, K ;

Lu, ZL ;

Duan, CY ;

Tian, YP ;

You, XZ .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 :1505-1507

[4]

MA YX, 1988, LANTHANIDE ACTINIDE, V2, P235

[5] PARST - A SYSTEM OF FORTRAN ROUTINES FOR CALCULATING MOLECULAR-STRUCTURE PARAMETERS FROM RESULTS OF CRYSTAL-STRUCTURE ANALYSES [J].

NARDELLI, M .

COMPUTERS & CHEMISTRY, 1983, 7 (03) :95-98

[6]

SHELDRICK G, 1993, SHELXL93 PROGRAM CRY

[7]

SHELDRICK GM, 1990, SHELXTL USER MANUAL

[8]

*SIEM, 1994, XSCANS US MAN VERS 2

[9] STRUCTURE OF 2-THIONYLTRIFLUOROACETONE ISONICOTINYL HYDRAZONE [J].

WANG, X ;

DENG, RW ;

WU, JG ;

CHEN, ZN .

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1992, 48 :1295-1297

[10]

WESTER D, 1973, J AM CHEM SOC, V95, P6506

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