Preparation and characterization of the nitramine-based energetic cocrystal composed of HMX and AP

被引：1

作者：

Zohari, Narges ^{[1
]}

Mohammadkhani, Faezeh Ghiasvand ^{[1
]}

Zabet, Zahra ^{[1
]}

Abrishami, Fatemeh ^{[1
]}

Hosseini, Seyed Ghorban ^{[1
]}

机构：

[1] Malek Ashtar Univ Technol, Fac Chem & Chem Engn, Tehran, Iran

来源：

JOURNAL OF ENERGETIC MATERIALS | 2024年 / 42卷 / 04期

关键词：

Cocrystallization; energetic materials; HMX; AP; AMMONIUM-PERCHLORATE; CO-CRYSTAL; SENSITIVITY; PERFORMANCE; EXPLOSIVES;

D O I：

10.1080/07370652.2022.2116502

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

In order to balance the contradiction between safety and performance of energetic compounds, a novel approach known as cocrystallization has been widely utilized. In this work, a novel cocrystal of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX) and ammonium perchlorate (AP) was successfully synthesized and characterized. The SEM images, PXRD spectra, and FT-IR spectrum confirmed the varied crystal structure of the cocrystal in comparison to the raw materials. In addition, the density of the cocrystal was measured to be 1.90 g.cm(-3), and the detonation velocity and detonation pressure were calculated to be (8.53) km.s(-1) and (35.21) GPa, respectively.

引用

页码：518 / 528

页数：11

共 36 条

[1] Crystal Engineering of Energetic Materials: Co-crystals of Ethylenedinitramine (EDNA) with Modified Performance and Improved Chemical Stability
Aakeroey, Christer B.
Wijethunga, Tharanga K.
Desper, John
[J]. CHEMISTRY-A EUROPEAN JOURNAL, 2015, 21 (31) : 11029 - 11037
[2] Aker?y B.P., 2012, SUPRAMOL CHEM, DOI [10.1002/9780470661345, DOI 10.1002/9780470661345.SMC113]
[3] Preparation of an Energetic-Energetic Cocrystal using Resonant Acoustic Mixing
Anderson, Stephen R.
Ende, David J. Am
Salan, Jerry S.
Samuels, Philip
[J]. PROPELLANTS EXPLOSIVES PYROTECHNICS, 2014, 39 (05) : 637 - 640
[4] Advances in science and technology of modern energetic materials: An overview
Badgujar, D. M.
Talawar, M. B.
Asthana, S. N.
Mahulikar, P. P.
[J]. JOURNAL OF HAZARDOUS MATERIALS, 2008, 151 (2-3) : 289 - 305
[5] SURFACE STRUCTURE OF AMMONIUM PERCHLORATE COMPOSITE PROPELLANTS
BOGGS, TL
DERR, RL
BECKSTEAD, MW
[J]. AIAA JOURNAL, 1970, 8 (02) : 370 - +
[6] High Power Explosive with Good Sensitivity: A 2:1 Cocrystal of CL-20:HMX
Bolton, Onas
Simke, Leah R.
Pagoria, Philip F.
Matzger, Adam J.
[J]. CRYSTAL GROWTH & DESIGN, 2012, 12 (09) : 4311 - 4314
[7] What is a co-crystal?
Bond, Andrew D.
[J]. CRYSTENGCOMM, 2007, 9 (09): : 833 - 834
[8] CRYSTAL STRUCTURE OF ALPHA-HMX AND A REFINEMENT OF STRUCTURE OF BETA-HMX
CADY, HH
CROMER, DT
LARSON, AC
[J]. ACTA CRYSTALLOGRAPHICA, 1963, 16 (07): : 617 - &
[9] [陈杰 Chen Jie], 2013, [含能材料, Chinese Jouranal of Energetic Materials], V21, P409
[10] Cocrystals of ammonium perchlorate with a series of crown ethers: preparation, structures, and properties
Cheng, Minmin
Liu, Xun
Luo, Qingping
Duan, Xiaohui
Pei, Chonghua
[J]. CRYSTENGCOMM, 2016, 18 (43): : 8487 - 8496

← 1 2 3 4 →