Al2O3-ZrO2Nanopowder Preparation By Polymer Gel-Net at Low Temperature

被引：5
作者：
Amirshaghaghi, Ahmad [1 ]
Kokabi, Mehrdad [1 ]
Keschtkar, Hossein Ali [1 ]
机构：
[1] Tarbiat Modares Univ, Dept Chem Engn, Polymer Engn Grp, Fac Engn, Tehran, Iran
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2010年 / 40卷 / 09期
关键词：
Al2O3-ZrO2; calcination; gel-net; nanopowders; ALUMINA-ZIRCONIA COMPOSITES; TRANSFORMATION BEHAVIOR; MECHANICAL-PROPERTIES; POWDER; MICROSTRUCTURE; CERAMICS; OXIDES; ZRO2; ZTA;
D O I：
10.1080/15533174.2010.509293
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The aim of this work was to produce alumina-zirconia nanopowder through the gel-net method at low temperature. The monomers acrylamide, N, N'-methylene-bis-acrylamide, persulphates and N,N,N',N'-tetra methyl ethyl diamine were used. The resultant network trapped and coordinated particles so that inhibited aggregation of Al2O3-ZrO2, improved homogeneity, decreased agglomeration and produced narrow particle size distribution of nanopowders. Complex formation between monomer and metal ions was investigated by Fourier transform infrared spectroscopy. Particle morphology and phase transformation during heat treatment were studied by scanning electron microscopy and X-ray diffraction, respectively. The nanopowders have spherical shape with particle sizes between 40 and 70 nm.
引用
收藏
页码：576 / 580
页数：5
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