2-Amino-4-(4-bromophenyl)-6-ferrocenylpyridine-3-carbonitrile

被引：1
作者：
Jia, Run-Hong
Tu, Shu-Jiang [1 ,2 ]
机构：
[1] Xuzhou Normal Univ, Coll Chem & Chem Engn, Xuzhou 221116, Peoples R China
[2] Lianyungang Teachers Coll, Lianyungang 222006, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词：
D O I：
10.1107/S160053680705489X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, [Fe(C5H5)(C17H11BrN3)], was synthesized by the reaction of 4-bromobenzaldehyde, acetylferrocene and ammonium acetate in an aqueous medium. The crystal packing is stabilized by intermolecular N-H center dot center dot center dot N hydrogen bonds. The dihedral angles between the phenyl ring and the pyridine and cyclopentadienyl rings are 51.67 (13) and 12.12 (21)degrees, respectively.
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页码：M135 / U1307
页数：9
相关论文
共 7 条
  • [1] The geometric features and spectral characteristics of some pentaamineruthenium(II) complexes
    Alyoubi, AO
    [J]. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2000, 56 (12) : 2397 - 2404
  • [2] *BRUK AXS INC, 1999, SAINT SHELXTL
  • [3] *BRUK AXS INC, 1998, SMART SADABS
  • [4] Desai JM, 2003, INDIAN J CHEM B, V42, P382
  • [5] METALLOCENES IN BIOCHEMISTRY, MICROBIOLOGY AND MEDICINE
    DOMBROWSKI, KE
    BALDWIN, W
    SHEATS, JE
    [J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1986, 302 (03) : 281 - 306
  • [6] Synthesis and structure-activity relationships of novel IKK-β inhibitors.: Part 3:: Orally active anti-inflammatory agents
    Murata, T
    Shimada, M
    Sakakibara, S
    Yoshino, T
    Masuda, T
    Shintani, T
    Sato, H
    Koriyama, Y
    Fukushima, K
    Nunami, N
    Yamauchi, M
    Fuchikami, K
    Komura, H
    Watanabe, A
    Ziegelbauer, KB
    Bacon, KB
    Lowinger, TB
    [J]. BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2004, 14 (15) : 4019 - 4022
  • [7] Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR, P38
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